N-(2,4-디메틸페닐)-2,4-디메틸벤젠아민

그림문자(GHS)

• 그림문자(GHS)

  

• 신호 어

  Warning

• 유해·위험 문구

  H315：피부에 자극을 일으킴

  H319：눈에 심한 자극을 일으킴

• 예방조치문구

  P264：취급 후에는 손을 철저히 씻으시오.

  P264：취급 후에는 손을 철저히 씻으시오.

  P280：보호장갑/보호의/보안경/안면보호구를 착용하시오.

  P302+P352：피부에 묻으면 다량의 물로 씻으시오.

  P305+P351+P338：눈에 묻으면 몇 분간 물로 조심해서 씻으시오. 가능하면 콘택트렌즈를 제거하시오. 계속 씻으시오.

  P332+P313：피부 자극이 생기면 의학적인 조치· 조언을 구하시오.

  P337+P313：눈에 대한 자극이 지속되면 의학적인 조치· 조언를 구하시오.

N-(2,4-디메틸페닐)-2,4-디메틸벤젠아민 화학적 특성, 용도, 생산

• 화학적 성질

  White powder

• 용도

  Bis(2,4-dimethylphenyl)amine is a pharmaceutical intermediate widely used in food, health care products, cosmetics and other fields.

• Synthesis

  2,4-dimethylaniline 2.67 g (molecular weight 121,22 mmol) was added to a 100 ml reaction flask under nitrogen.2.68 g of 2,4-dimethylbromobenzene (molecular weight 184,20 mmol), 5.76 g of sodium tert-butoxide (molecular weight 96,60 mmol), Pd2(dba)3 183 mg (molecular weight 916, 0.2 mmol), P(tBu)3 121 mg (molecular weight 202, 0.6 mmol).Anhydrous toluene 50 ml.After the addition, the oil bath was slowly heated to reflux reaction, and TLC monitored the reaction end, and the reaction was completed in 10 hours. Cooled, quenched with water, and extracted with 50ml of dichloromethane, the organic phase dried over anhydrous MgSO4, and the organic phase evaporated to dryness; the resulting solid was separated by column chromatography to give a white solid Bis(2,4-dimethylphenyl)amine 3.8g, molecular weight 225, 85percent yield.

N-(2,4-디메틸페닐)-2,4-디메틸벤젠아민 공급 업체

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