N-メチル-N-トリメチルシリルメチル-N′-TERT-ブチルホルムアミジン

N-メチル-N-トリメチルシリルメチル-N′-TERT-ブチルホルムアミジン 化学特性,用途語,生産方法

• 化学的特性

  CLEAR PALE YELLOW LIQUID

• 使用

  N-METHYL-N-TRIMETHYLSILYLMETHYL-N'-TERT-BUTYLFORMAMIDINE conveniently effects the transformation of ketones and aldehydes to homologated nitriles, amines, aldehydes, and ketones.

• 合成

  N-METHYL-N-TRIMETHYLSILYLMETHYL-N'-TERT-BUTYLFORMAMIDINE is easily synthesized by a two-step procedure (eq 1).1 Initially, the condensation of t-Butylamine with either N,N-Dimethylformamide or dimethylformamide dimethyl acetal cleanly affords N′-t-Butyl-N,N-dimethylformamidine. Subsequent lithiation and silylation with Chlorotrimethylsilane results in a 70% overall yield of the purified title reagent.
  

• 貯蔵

  The reagent should be handled in a fume hood. Refrigeration should be used for prolonged storage.

N-メチル-N-トリメチルシリルメチル-N′-TERT-ブチルホルムアミジン 生産企業

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