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2-Bromo-3-methylaniline

2-Bromo-3-methylaniline Structure
2-Bromo-3-methylaniline
  • CAS No.54879-20-8
  • Chemical Name:2-Bromo-3-methylaniline
  • CBNumber:CB9498840
  • Molecular Formula:C7H8BrN
  • Formula Weight:186.05
  • MOL File:54879-20-8.mol
2-Bromo-3-methylaniline Property
  • Boiling point 48 °C/0.03 mmHg (lit.)
  • Density 1.489 g/mL at 25 °C (lit.)
  • refractive index n20/D 1.605(lit.)
  • Flash point >230 °F
  • storage temp. Keep in dark place,Sealed in dry,Room Temperature
  • form Liquid
  • pka 2.66±0.10(Predicted)
  • color Pale brown
  • UNSPSC Code 12352100
Safety
Hazard and Precautionary Statements (GHS)
  • Symbol(GHS)
  • Signal wordWarning
  • Hazard statements H302-H317
  • Precautionary statements P280-P301+P312+P330-P302+P352
2-Bromo-3-methylaniline Price More Price(1)
  • Brand: Sigma-Aldrich(India)
  • Product number: 645621
  • Product name : 2-Bromo-3-methylaniline
  • Purity: 98%
  • Packaging: 5G
  • Price: ₹37281.3
  • Updated: 2022/06/14
  • Buy: Buy

2-Bromo-3-methylaniline Chemical Properties,Usage,Production

  • Synthesis Add iron powder (3.86 g, 69 mmol), water (5 mL) and concentrated HCL (0.5 mL) sequentially to a solution of commercially available 2-bromo-3-nitrotoluene (5 g, 23 mmol) in methanol (100 mL) at room temperature and heat the mixture at reflux for 125 h. Remove the solvents under reduced pressure, suspend the residue in water (400 mL) and extract with chloroform (3 x 250 mL). Dry the combined organic extracts over MGS04 and remove the solvents under reduced pressure to afford 2-bromo-3-methylphenylamine as an amber oil (4.45 g, 100percent): 1H NMR (CDC13) 5 2.30 (s, 3H), 4.00 (br s, 2H), 7.60 (m, 2H), 7.00 (t, 1H).
2-Bromo-3-methylaniline Preparation Products And Raw materials
Raw materials
Preparation Products
2-Bromo-3-methylaniline Suppliers
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2-Bromo-3-methylaniline Spectrum
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