Preparation
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METHYL 3-METHOXY-4-METHYLBENZOATE

Preparation
METHYL 3-METHOXY-4-METHYLBENZOATE Structure
METHYL 3-METHOXY-4-METHYLBENZOATE
  • CAS No.3556-83-0
  • Chemical Name:METHYL 3-METHOXY-4-METHYLBENZOATE
  • CBNumber:CB9372636
  • Molecular Formula:C10H12O3
  • Formula Weight:180.2
  • MOL File:3556-83-0.mol
METHYL 3-METHOXY-4-METHYLBENZOATE Property
  • Melting point 50-54 °C (lit.)
  • Boiling point 119-120°C 1mm
  • Density 1.075±0.06 g/cm3(Predicted)
  • refractive index 1.5295
  • Flash point >230 °F
  • form powder to crystal
  • color White to Almost white
  • BRN 1948339
  • CAS DataBase Reference 3556-83-0(CAS DataBase Reference)
  • UNSPSC Code 12352100
  • NACRES NA.22
Safety
  • Hazard Codes  :Xi
  • Risk Statements  :36/37/38
  • Safety Statements  :26-36
  • WGK Germany  :1
  • HS Code  :29189900
  • NFPA 704:
    1
    0 0
Hazard and Precautionary Statements (GHS)
  • Symbol(GHS)
  • Signal wordWarning
  • Hazard statements H315-H319-H335
  • Precautionary statements P261-P264-P271-P280-P302+P352-P305+P351+P338
METHYL 3-METHOXY-4-METHYLBENZOATE Price More Price(3)
  • Brand: Sigma-Aldrich(India)
  • Product number: 528781
  • Product name : Methyl 3-methoxy-4-methylbenzoate
  • Purity: 96%
  • Packaging: 25G
  • Price: ₹20924.73
  • Updated: 2022/06/14
  • Buy: Buy
  • Brand: TCI Chemicals (India)
  • Product number: M1427
  • Product name : Methyl 3-Methoxy-4-methylbenzoate
  • Purity: min. 98.0 %
  • Packaging: 5G
  • Price: ₹3800
  • Updated: 2022/05/26
  • Buy: Buy
  • Brand: TCI Chemicals (India)
  • Product number: M1427
  • Product name : Methyl 3-Methoxy-4-methylbenzoate
  • Purity: min. 98.0 %
  • Packaging: 25G
  • Price: ₹9000
  • Updated: 2022/05/26
  • Buy: Buy

METHYL 3-METHOXY-4-METHYLBENZOATE Chemical Properties,Usage,Production

  • Preparation Methyl 3-methoxy-4-methylbenzoate is synthesized by the following steps:A mixture of methyl 3-hydroxy-4-methylbenzoate 36 (25 g, 0.151 mol),  Me2SO4 (28.3 ml, 0.386 mol), anhydrous K2CO3 (103.5 g, 0.75 mol) was  refluxed in acetone for 2 hours. K2CO3 was filtered off, washed  thoroughly with acetone. The filtrates were combined and concentrated,  the residue was redissolved in EtOAc washed with water, dried  (anhydrous Na2SO4), filtered and concentrated in vacuo to furnish a white solid (19.52 g).  Yield : 72%.
  • Chemical Properties White low melting solid
  • Uses Methyl 3-Methoxy-4-methylbenzoate has been used as a reactant in the preparation of an antimalaria drug that consists of the 4-aminoquinoline pharmacophore of chloroquine with clotrimazole-based antimalarials.
  • Synthesis Reference(s) Journal of Medicinal Chemistry, 33, p. 1771, 1990 DOI: 10.1021/jm00168a036
  • General Description Methyl 3-methoxy-4-methylbenzoate can be prepared by reacting diazomethane with 3-methoxy-4-methylbenzoic acid in ether.
METHYL 3-METHOXY-4-METHYLBENZOATE Preparation Products And Raw materials
Raw materials
Preparation Products
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METHYL 3-METHOXY-4-METHYLBENZOATE Spectrum
3556-83-0, METHYL 3-METHOXY-4-METHYLBENZOATERelated Search:
  • C10 to C11
  • Aromatic Esters
  • Anisoles, Alkyloxy Compounds & Phenylacetates
  • Acids & Esters
  • Esters
  • Carbonyl Compounds
  • 化工原料及中间体
  • 系列1
  • 高端化学
  • 苯环类
  • 医药中间体
  • 通用试剂
  • 有机砌块
  • 酯
  • C10 to C11
  • Carbonyl Compounds
  • Building Blocks
  • Esters
  • Organic Building Blocks
  • CH3OC6H3CH3CO2CH3
  • 3-甲氧基-4-甲基苯甲甲氧基-4-甲基苯甲酸甲酯
  • 4-甲基-3-甲氧基苯甲酸甲酯
  • 3-甲氧基-4-甲基安息香酸甲酯
  • 3-甲氧基-4-甲基苯甲酸甲酯
  • 3-甲氧基-4-甲基苯甲酸甲
  • 3-甲氧基-4-甲基苯甲酸甲酯,98%
  • 4-甲基-3-甲氧基苯甲酯
  • 3-甲氧基-4-甲基苯甲酸甲,98%
  • 3556-83-0
  • 3-Methoxy-4-methylbenzoate methyl ester
  • 3-Methoxy-4-Methylbenzoic Acid Methyl Easter
  • Methyl3-Methoxy-4-methylbenzoate&gt
  • 3-METHOXY-P-TOLUIC ACID METHYL ESTER
  • 3-METHOXY-4-METHYLBENZOIC ACID METHYL ESTER
  • METHYL 4-METHYL-M-ANISATE
  • 4-METHYL-M-ANISIC ACID METHYL ESTER
  • Methyl 4-methyl-3-(methyloxy)benzoate
  • 3-Methoxy-4-methylbenzoic Acid Methyl Ester 3-Methoxy-p-toluic Acid Methyl Ester 4-Methyl-m-anisic Acid Methyl Ester Methyl 3-Methoxy-p-toluate Methyl 4-Methyl-m-anisate
  • Benzoic acid, 3-Methoxy-4-Methyl-, Methyl ester
  • Methyl 3-methoxy-4-methylbenzoate, 98+%
  • 4-METHOXY-3-METHYLBENZOIC ACID METHYL ESTER
  • 3-Methoxy-4-methyl-benzoesuremethylester
  • METHYL 3-METHOXY-4-METHYLBENZOATE
  • METHYL 3-METHOXY-P-TOLUATE

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