ChemicalBook > CAS DataBase List > 1-(Triisopropylsilyl)-1H-pyrrolo[2,3-b]pyridin-5-ol

1-(Triisopropylsilyl)-1H-pyrrolo[2,3-b]pyridin-5-ol

1-(Triisopropylsilyl)-1H-pyrrolo[2,3-b]pyridin-5-ol Structure
1-(Triisopropylsilyl)-1H-pyrrolo[2,3-b]pyridin-5-ol
  • CAS No.685514-01-6
  • Chemical Name:1-(Triisopropylsilyl)-1H-pyrrolo[2,3-b]pyridin-5-ol
  • CBNumber:CB81871753
  • Molecular Formula:C16H26N2OSi
  • Formula Weight:290.48
  • MOL File:685514-01-6.mol
1-(Triisopropylsilyl)-1H-pyrrolo[2,3-b]pyridin-5-ol Property
  • Boiling point 341.6±35.0 °C(Predicted)
  • Density 1.03±0.1 g/cm3(Predicted)
  • pka 8.50±0.40(Predicted)
Hazard and Precautionary Statements (GHS)
  • Symbol(GHS)
  • Signal wordWarning
  • Hazard statements H302-H315-H319-H335
  • Precautionary statements P261-P264-P270-P271-P280-P301+P312-P302+P352-P304+P340-P305+P351+P338-P330-P332+P313-P337+P313-P362-P403+P233-P405-P501

1-(Triisopropylsilyl)-1H-pyrrolo[2,3-b]pyridin-5-ol Chemical Properties,Usage,Production

  • Synthesis Add 10.8g (34mmol) of (1-(triisopropylsilyl)-1H-pyrrolo[2,3-b]pyridin-5-yl)boronic acid and 120mL of tetrahydrofuran to a round bottom flask equipped with a magnetic stirrer, an inert gas source and a separating funnel, and stir to dissolve; Add 34mL of 1mol/L sodium hydroxide solution and 4.60g (40.6mmol) of 30% hydrogen peroxide dropwise at 0°C. After the addition, React at 0°C for 1 hour and detect the reaction by TLC. Add 4.8g (20.24mmol) of sodium thiosulfate, adjust to pH=5 with 2mol/L hydrochloric acid, extract with ethyl acetate (2x200mL), combine the organic phases, wash with saturated brine in turn, dry with a sodium sulfate, and reduce Concentrate under pressure. The residue was purified by silica gel column chromatography [eluent: dichloromethane] to obtain 1-(Triisopropylsilyl)-1H-pyrrolo[2,3-b]pyridin-5-ol 9.4g, yield 95.0%.
    1H-Pyrrolo[2,3-b]pyridin-5-ol, 1-[tris(1-methylethyl)silyl]-
1-(Triisopropylsilyl)-1H-pyrrolo[2,3-b]pyridin-5-ol Preparation Products And Raw materials
Raw materials
Preparation Products
1-(Triisopropylsilyl)-1H-pyrrolo[2,3-b]pyridin-5-ol Suppliers
Global(48)Suppliers
  • Supplier：
    career henan chemical co
  • Tel：+86-0371-86658258<br/>+8613203830695
  • Email：factory@coreychem.com
  • Country：China
  • ProdList：29808
  • Advantage：58
  • Supplier：
    Labnetwork lnc.
  • Tel：+86-27-50766799<br/>+8618062016861
  • Email：contact@labnetwork.com
  • Country：China
  • ProdList：19987
  • Advantage：58
  • Supplier：
    Alfa Chemistry
  • Tel：
  • Email：Info@alfa-chemistry.com
  • Country：United States
  • ProdList：24072
  • Advantage：58
  • Supplier：
    LEAPCHEM CO., LTD.
  • Tel：+86-852-30606658
  • Email：market18@leapchem.com
  • Country：China
  • ProdList：43340
  • Advantage：58
1-(Triisopropylsilyl)-1H-pyrrolo[2,3-b]pyridin-5-ol Spectrum
685514-01-6, 1-(Triisopropylsilyl)-1H-pyrrolo[2,3-b]pyridin-5-olRelated Search:
  • 有机中间体
  • C16H26N2OSi
  • 1-(三异丙基甲硅烷基)-1H-吡咯并[2,3-B]吡啶-5-酚
  • 1-三异丙基硅基-5-羟基-7-氮杂吲哚
  • 1-(三异丙基硅烷基)-1H-吡咯并[2,3-B]吡啶-5-醇
  • 685514-01-6
  • 1-(triisopropylsilyl)-1H-pyrrolo[2,3-b]pyridin-5-ol
  • 1-Triisopropylsilanyl-1H-pyrrolo[2,3-b]pyridin-5-ol
  • 1-tri(propan-2-yl)silylpyrrolo[2,3-b]pyridin-5-ol
  • 1-[tris(propan-2-yl)silyl]-1H-pyrrolo[2,3-b]pyridin-5-ol
  • 1-[(2-methylpropan-2-yl)oxycarbonyl]piperidine-4-sulfonic acid
  • 1-triisopropylsilylpyrrolo[2,3-b]pyridin-5-ol
  • 1-[Tris(1-methylethyl)silyl]-1H-pyrrolo[2,3-b]pyridin-5-ol
  • 1H-Pyrrolo[2,3-b]pyridin-5-ol, 1-[tris(1-methylethyl)silyl]-

Home

My