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3-Amino-4-methoxybenzanilide

3-Amino-4-methoxybenzanilide Structure
3-Amino-4-methoxybenzanilide
  • CAS No.120-35-4
  • Chemical Name:3-Amino-4-methoxybenzanilide
  • CBNumber:CB7251074
  • Molecular Formula:C14H14N2O2
  • Formula Weight:242.27
  • MOL File:120-35-4.mol
3-Amino-4-methoxybenzanilide Property
  • Melting point 154-156°C
  • Boiling point 385.1°C (rough estimate)
  • Density 1.1338 (rough estimate)
  • vapor pressure 0-0Pa at 25℃
  • refractive index 1.6419 (estimate)
  • storage temp. Keep in dark place,Inert atmosphere,Room temperature
  • solubility DMSO (Slightly), Methanol (Slightly)
  • form Solid
  • pka 13.44±0.70(Predicted)
  • color White to Off-White
  • LogP 2.08 at 23℃ and pH7
  • CAS DataBase Reference 120-35-4(CAS DataBase Reference)
  • FDA UNII V5Y646AW8S
  • EPA Substance Registry System Benzamide, 3-amino-4-methoxy-N-phenyl- (120-35-4)
Safety
  • Risk Statements  :36/37/38
  • Safety Statements  :26-36/37/39
  • RTECS  :CV7400000
  • TSCA  :Yes
  • HazardClass  :IRRITANT
  • HS Code  :2924297099
  • Toxicity :mouse,LD50,intravenous,320mg/kg (320mg/kg),U.S. Army Armament Research & Development Command, Chemical Systems Laboratory, NIOSH Exchange Chemicals. Vol. NX#01183,
  • NFPA 704:
    0
    0 0
Hazard and Precautionary Statements (GHS)
  • Symbol(GHS)
  • Signal wordWarning
  • Hazard statements H315-H319-H335
  • Precautionary statements P261-P305+P351+P338
3-Amino-4-methoxybenzanilide Price More Price(1)
  • Brand: TCI Chemicals (India)
  • Product number: A1954
  • Product name : 3-Amino-4-methoxybenzanilide
  • Purity: 
  • Packaging: 25G
  • Price: ₹5200
  • Updated: 2022/05/26
  • Buy: Buy

3-Amino-4-methoxybenzanilide Chemical Properties,Usage,Production

  • Chemical Properties Gray powder.
  • Uses 3-Amino-4-methoxybenzanilide is used in preparation method of Cyanate resin-based near-zero expansion composite material truss rod.
  • Uses Dyes, pharmaceuticals, and other organic chemicals.
  • Synthesis 3-Amino-4-methoxybenzanilide is prepared by the reaction of 3-amino-4-methoxybenzoic acid and aniline. The steps are as follows:
    A total of 0.17 mL (0.18 mmol) of DIC and 0.24 g (0.18 mmol) of HOBt were added to a dichloromethane solution of 0.20 g (0.12 mmol) of 1 at room temperature, and the reaction mixture was stirred for 0.5 h. Then, 0.13 mL (0.14 mmol) of aniline was added to the mixture. After approximately 3 h, 0.5 N NaOH was added to the solution. The lower layer was isolated, and 0.5 N HCl was added until the aqueous solution was neutral. The dichloromethane layer was washed three times with 10 mL of water, and then MgSO4 was added. After 2 h, the solution was filtered, and the solvent was removed. The residue was purified by column chromatography on silica gel (eluent: petroleum ether:ethyl acetate = 3:1) to yield the desired 3-Amino-4-methoxybenzanilide as a white solid (yield: 76%). Mp: 197-198 °C. 1H NMR (400 MHz, DMSO-d6) δ (ppm): 9.92 (1H, s, NH), 7.74 (2H, d, J = 9.0 Hz, PhH), 7.32 (2H, m, PhH), 7.21 (2H, d, J = 8.0 Hz, PhH), 7.06 (1H, m, PhH), 6.88 (1H, d, J = 8.0 Hz, PhH), 4.90 (2H, br s, NH2), 3.83 (3H, s, OCH3). ESI-MS (m/z): 243 (M + H)+.
    3-Amino-4-methoxybenzanilide synthesis
3-Amino-4-methoxybenzanilide Preparation Products And Raw materials
Raw materials
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3-Amino-4-methoxybenzanilide Spectrum
120-35-4, 3-Amino-4-methoxybenzanilideRelated Search:
  • Aromatic Carboxylic Acids, Amides, Anilides, Anhydrides & Salts
  • Intermediates of Dyes and Pigments
  • 高端化学
  • 其它原料及中间体
  • 有机类
  • 化工
  • 对照品
  • 有机化工原料
  • 化工原料
  • 助剂
  • 药物杂质及中间体
  • 有机中间体
  • 色基
  • 染料
  • 冰染染料
  • 酰胺/酰胺化合物
  • 有机砌块
  • 有机颜料中间体
  • 芳烃
  • 酰胺化合物
  • 酰胺
  • 红色基 KD(3-氨基-4-甲氧基-苯酰替苯胺 )
  • 红色基KD 3-氨基-4-甲氧基苯甲酰苯胺
  • 红色基KD(DB-40)
  • 3-氨基-4-甲氧基萘氨(CAS号:120-35-4)
  • 4-甲氧基-3-氨基苯酰替苯胺(红色基KD)
  • 红色基 KD
  • 3-氨基-4-甲氧基苯甲酰替苯胺红色基KD (DB-40)
  • 3-氨基-4-甲氧基苯甲酰苯胺
  • 耐晒红KD
  • 3-氨基对茴香苯胺
  • 3-氨基-4-甲氧基-N-苯基苯甲酰胺,98%
  • 3-氨基-4-甲氧基萘氨,98%
  • 4-甲氧基-3-氨基苯酰替苯胺
  • 3-氨基-4-甲氧基萘氨
  • 3-氨基-4-甲氧基-N-苯基苯甲酰胺
  • 120-35-4
  • Red based KD
  • 3-Amino-4-methoxybenzanilide 120-35-4
  • DB-40 (3-AMINO-4-METHOXYBENZANILIDE )
  • 3-Amino-4-methoxybenzanilide ISO 9001：2015 REACH
  • Red KD Base
  • 3-Amino-4-methoxybenzanilide &gt
  • Benzamide,3-amino-4-methoxy-N-phenyl-
  • 1-hydroxy-6,8a-dimethylspiro[4a,6,7,8-tetrahydro-4H-naphthalene-5,2'-oxirane]-1,2-dicarboxaldehyde
  • 3-amino-4-methoxy-n-phenyl-benzamid
  • 3-amino-4-methoxy-benzanilid
  • N-Phenyl-4-methoxy-3-aminobenzamide
  • 4-Methoxy-3-aminobenzanilide
  • N-(3-amino-4-methoxyphenyl)benzamide
  • 3-Amino-p-anisanilide,prac.,95%
  • FAST RED KD BASE
  • LABOTEST-BB LT01138545
  • 3-AMINO-P-ANISANILIDE
  • 3-AMINO-4-METHOXY-N'-PHENYL BENZAMIDE
  • 3-AMINO-4-METHOXYBENZANILIDE
  • AMBA
  • AMAN

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