ChemicalBook > CAS DataBase List > 2,5-Dibromo-3-nitropyridine
2,5-Dibromo-3-nitropyridine
2,5-Dibromo-3-nitropyridine
- CAS No.15862-37-0
- Chemical Name:2,5-Dibromo-3-nitropyridine
- CBNumber:CB1947685
- Molecular Formula:C5H2Br2N2O2
- Formula Weight:281.89
- MOL File:15862-37-0.mol
2,5-Dibromo-3-nitropyridine Property
- Melting point 92.0 to 96.0 °C
- Boiling point 272.7±35.0 °C(Predicted)
- Density 2?+-.0.06 g/cm3(Predicted)
- storage temp. under inert gas (nitrogen or Argon) at 2–8 °C
- solubility soluble in Methanol
- pka -5.60±0.20(Predicted)
- form Solid
- color Yellow
- InChIKey OQKWPJCAKRVADO-UHFFFAOYSA-N
- CAS DataBase Reference 15862-37-0(CAS DataBase Reference)
- UNSPSC Code 12352200
Safety
-
Symbol(GHS)
- Signal wordDanger
- Hazard statements H301
- Precautionary statements P301+P310
2,5-Dibromo-3-nitropyridine Price
More Price(6)
- Brand: Sigma-Aldrich(India)
- Product number: ADE000413
- Product name : 2,5-Dibromo-3-nitro-pyridine
- Purity: AldrichCPR
- Packaging: 1G
- Price: ₹62795.83
- Updated: 2022/06/14
- Buy: Buy
- Brand: ALFA India
- Product number: ALF-H61961-22
- Product name : 2,5-Dibromo-3-nitropyridine, 98%
- Purity:
- Packaging: 100g
- Price: ₹26312
- Updated: 2022/05/26
- Buy: Buy
- Brand: TCI Chemicals (India)
- Product number: D4702
- Product name : 2,5-Dibromo-3-nitropyridine
- Purity: min. 98.0 %
- Packaging: 1G
- Price: ₹1500
- Updated: 2022/05/26
- Buy: Buy
- Brand: TCI Chemicals (India)
- Product number: D4702
- Product name : 2,5-Dibromo-3-nitropyridine
- Purity: min. 98.0 %
- Packaging: 5G
- Price: ₹2700
- Updated: 2022/05/26
- Buy: Buy
- Brand: ALFA India
- Product number: ALF-H61961-14
- Product name : 2,5-Dibromo-3-nitropyridine, 98%
- Purity:
- Packaging: 25g
- Price: ₹21937
- Updated: 2022/05/26
- Buy: Buy
2,5-Dibromo-3-nitropyridine Chemical Properties,Usage,Production
- Uses 2,5-Dibromo-3-nitropyridine is used as organic synthesis intermediate and pharmaceutical intermediate, mainly used in laboratory research and development process and chemical production process.
-
Preparation
synthesis of 2,5-Dibromo-3-nitropyridine: To a suspension 5-bromo-3-nitro-pyridin-2-ol (20 g, 91.32 mmol) in toluene (100 ml) was added DMF (0.7 ml, 9.13 mmol) and the mixture was heated to 90??C. (the reaction mixture was protected from light). A solution of POBr3 (31. 41 g, 109.51 mmol) in toluene (40 ml) was added dropwise at 90??C. and the reaction mixture was stirred at that temperature for 16 h. The mixture was allowed to cool to room temperature and toluene (50 ml) and water (50 ml) were added. The organic layer was separated, washed successively with aqueous 1N NaOH (60 ml), water (60 ml) and brine (30 ml), dried with Na2SO4 and evaporated obtain 2,5-Dibromo-3-nitropyridine. Yellow solid, yield 25.2 g, 97%.
2,5-Dibromo-3-nitropyridine Preparation Products And Raw materials
Raw materials
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15862-37-0, 2,5-Dibromo-3-nitropyridineRelated Search:
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- 化工中间体
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- 高端化学
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- 吡啶类衍生物
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- 2,5-Dibromo-3-nitropyridine,98%
- 2,5-Dibromo-3-nitropyridine >
- 2,5-<WBR>DibroMo-<WBR>3-<WBR>nitro-<WBR>pyridine
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- 2,5-Dibromo-3-nitropyridi...
- 2,5-Dibromo-3-nitropyridine ,97%
- Nsc170627
- 2,5-Dibromo-3-nitropyridine