3-Bromophenylmethylsulfone

Gefahreninformationscode (GHS)

• Bildanzeige (GHS)

  

• Alarmwort

  Warnung

• Gefahrenhinweise

  H315：Verursacht Hautreizungen.

  H319：Verursacht schwere Augenreizung.

• Sicherheit

  P264：Nach Gebrauch gründlich waschen.

  P264：Nach Gebrauch gründlich waschen.

  P280：Schutzhandschuhe/Schutzkleidung/Augenschutz tragen.

3-Bromophenylmethylsulfone Chemische Eigenschaften,Einsatz,Produktion Methoden

• Chemische Eigenschaften

  White Solid

• Synthese

  3-Bromothioanisole (8.7 g, 43 mmol) was added to dichloromethane (125 mL) to it and cooled to 0C. To this was added 3-chloroperbenzoic acid (22.2 g, 129 mmol). m- CPBA was not completely dissolved. The reaction mixture was stirred overnight. The reaction was purged with saturated thiosulfate sodium (150 mL) solution to quench it. The product was extracted with EtOAc (3 x 100 mL). The organic fractions portions were combined, washed with brine (75 mL) and dried over sodium sulfate. The organic liquids were then concentrated to give 9.89 g (97%) of 3-bromophenyl methyl sulfone.

3-Bromophenylmethylsulfone Anbieter Lieferant Produzent Hersteller Vertrieb Händler.

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