349120-88-3

Wash the round bottom flask properly and rinse with  distilled water. Add 10 ml of 10% solution of sodium carbonate in round bottom flask  and 0.1 ml of 2,5-dimethyl aniline. Shake it well to mix it evenly. Gradually add 1 ml 0f acid in  the flask and shake it vigorously. Filter the reaction as the precipitates appeared. Precipitates  were dried and confirmed by performing TLC. Amount of obtained product was  calculated and saved.