14180-63-3

Preparative Method of Diallyl Sulfoxide: conveniently prepared in 91% yield from commercially available diallyl sulfide by oxidation with 30% H2O2 in acetone at rt followed by recrystallization at -20 °C from pentane/ether.^[1]

Tetrahedron Letters, 21, p. 689, 1980 DOI: 10.1016/S0040-4039(00)71446-8

1. Block, E.; Zhao, S.-H. TL 1990, 31, 5003.