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• Synthesis

  The protected amino acid derivative (2 mg) was placed in a 1.5 mL glass vial with a screw cap. The appropriate acid solution (1 mL) and 0.1 M HCl were added to the HFIP. The reaction mixture was incubated at room temperature for 240 min, and the product Fmoc-Lys-OH hydrochloride was obtained by RT-HPLC and MALDI-TOF or ESI HR mass spectrometry.

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