图谱信息 供应商 相关产品
网站主页CAS数据库列表 99-71-8更多图谱4-仲丁基苯酚(99-71-8)核磁图(1HNMR)

4-仲丁基苯酚

产品名称 4-仲丁基苯酚

CAS号99-71-8

分子式C10H14O

分子量150.22

展开


  • Mass

    MS-NW-1821          
    p-sec-butylphenol
    C10H14O             (Mass of molecular ion:    150)
    

       Source Temperature: 250 °C
       Sample Temperature: 180 °C
       Reservoir, 75 eV
    

          27.0       3.0
          29.0       1.8
          39.0       5.3
          41.0       2.9
          51.0       2.9
          53.0       1.6
          55.0       1.9
          63.0       2.0
          65.0       5.0
          66.0       1.2
          77.0      12.7
          78.0       1.9
          79.0       1.3
          91.0       9.6
          92.0       1.5
          93.0       4.3
          94.0       1.6
          95.0       1.1
         103.0       8.6
         107.0      11.0
         119.0       1.7
         120.0       3.0
         121.0     100.0
         122.0       8.9
         135.0       3.9
         150.0      17.5
         151.0       1.9
    

90 MHz in CDCl3


  • 1H NMR 89.56 MHz
    C10 H14 O 0.041 g : 0.5 ml CDCl3
    p-sec-butylphenol
    ChemicalStructure
        Assign.     Shift(ppm)
    A 7.026 B 6.763 C 4.93 D 2.51 E 1.54 F 1.195 G 0.81 J(F,D)=6.9HZ.

         Hz     ppm     Int.
    

        635.00   7.091    222
        634.63   7.087    227
        632.75   7.066     86
        628.56   7.019    106
        628.19   7.015    100
        626.25   6.993    466
        623.69   6.964     67
        611.25   6.826     76
        608.63   6.796    570
        606.38   6.771    134
        602.19   6.724     97
        599.94   6.699    293
        444.38   4.962     32
        443.63   4.954     36
        442.19   4.938     43
        441.81   4.934     44
        441.44   4.929     44
        440.75   4.922     44
        440.38   4.918     43
        439.75   4.911     42
        237.25   2.650     38
        230.19   2.571     82
        223.19   2.493     92
        216.25   2.415     55
        153.50   1.714     35
        152.63   1.705     33
        146.81   1.640     68
        145.44   1.624    180
        138.31   1.545    188
        137.81   1.539    200
        131.88   1.473    103
        130.94   1.463    220
        124.50   1.391     58
        123.88   1.384     54
        110.19   1.231   1000
        108.19   1.209     39
        103.31   1.154    847
        101.25   1.131     34
         78.69   0.879    322
         71.94   0.804    565
         71.19   0.795    378
         64.19   0.717    189
         63.25   0.707    106
    

in CDCl3



CCl4 solution



KBr disc



liquid film



nujol mull