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1,3-二氯丙醇

产品名称 1,3-二氯丙醇

CAS号96-23-1

分子式C3H6Cl2O

分子量128.99

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  • Mass

    MS-NW-4341          
    1,3-dichloro-2-propanol
    C3H6Cl2O            (Mass of molecular ion:    128)
    

       Source Temperature: 240 °C
       Sample Temperature: 180 °C
       Reservoir, 75 eV
    

          15.0       7.2
          26.0       1.4
          27.0       4.7
          29.0       4.3
          31.0       3.8
          36.0       1.4
          37.0       1.0
          38.0       1.3
          39.0       3.2
          41.0       1.0
          42.0       2.9
          43.0      37.5
          44.0       2.4
          48.0       1.1
          49.0       8.3
          50.0       1.2
          51.0       2.9
          57.0       1.2
          61.0       1.2
          62.0       2.8
          64.0       1.2
          75.0       1.7
          78.0       2.0
          79.0     100.0
          80.0       2.9
          81.0      33.9
    

90 MHz in CDCl3

parameter in CDCl3


  • 1H NMR 89.56 MHz
    C3 H6 Cl2 O 0.04 ml : 0.5 ml CDCl3
    1,3-dichloro-2-propanol
    ChemicalStructure
        Assign.     Shift(ppm)
    A 4.072 B 3.697 C 2.6 J(A,B)=5.2HZ. CONFIRMED BY LAOCN PROGRAM.

         Hz     ppm     Int.
    

        371.63   4.150     23
        370.38   4.136     70
        367.19   4.100     28
        365.50   4.082     99
        364.75   4.073     78
        361.75   4.040     34
        359.88   4.019    120
        355.13   3.966     70
        333.44   3.724   1000
        328.50   3.668    638
        233.38   2.606     47
    


  • 1H NMR 300 MHz
    C3 H6 Cl2 O 0.04 ml : 0.5 ml CDCl3
    1,3-dichloro-2-propanol
    ChemicalStructure
        Parameter     ppm  Hz
    D(A) 4.072 D(B) 3.697 J(A,B) 5.24 D(C) 2.61

         Hz     ppm     Int.
    

       1232.31   4.108     27
       1226.98   4.090     99
       1221.78   4.073    154
       1216.51   4.055    118
       1211.40   4.038     39
       1111.66   3.706   1000
       1106.44   3.688    897
        783.00   2.610     29
    

in CDCl3



liquid film