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网站主页CAS数据库列表 92-05-7更多图谱联苯-3,4-二醇(92-05-7)红外图谱(IR2)

联苯-3,4-二醇

产品名称 联苯-3,4-二醇

CAS号92-05-7

分子式C12H10O2

分子量186.21

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  • Mass

    MS-IW-3860          
    4-phenylpyrocatechol
    C12H10O2            (Mass of molecular ion:    186)
    

       Source Temperature: 150 °C
       Sample Temperature: 110 °C
       Direct, 75 eV
    

          18.0       1.5
          39.0       1.0
          50.0       1.1
          51.0       2.7
          62.0       1.1
          63.0       2.1
          64.0       1.4
          69.0       1.5
          69.5       2.7
          70.0       3.6
          74.0       1.0
          75.0       1.2
          77.0       2.1
          78.0       1.2
          89.0       1.2
          93.0       5.1
         102.0       1.4
         113.0       1.0
         114.0       1.4
         115.0       2.3
         127.0       2.2
         128.0       4.4
         129.0       2.2
         138.0       1.1
         139.0      20.9
         140.0      13.8
         141.0       2.0
         157.0       4.2
         168.0       1.1
         170.0       1.8
         185.0       2.5
         186.0     100.0
         187.0      13.2
         188.0       1.2
         220.0       2.8
    

400 MHz in DMSO-d6


  • 1H NMR 399.65 MHz
    C12 H10 O2 0.035 g : 0.5 ml DMSO-d6
    4-phenylpyrocatechol
    ChemicalStructure
        Assign.     Shift(ppm)
    A *1 9.08 B *1 9.05 C 7.527 D 7.394 E 7.263 F 7.069 G 6.947 J 6.847 J(F,G)=2.3HZ J(G,J)=8.2HZ

         Hz     ppm     Int.
    

       3628.91   9.081    315
       3617.31   9.052    307
       3013.67   7.541    567
       3012.45   7.538    712
       3010.38   7.533    224
       3005.25   7.520    908
       3004.03   7.517    792
       3002.20   7.513    161
       2998.66   7.504     42
       2976.32   7.448     35
       2967.53   7.426     42
       2963.01   7.415    531
       2961.06   7.410    187
       2959.35   7.405     74
       2955.57   7.396    861
       2949.22   7.380    225
       2947.63   7.376    517
       2945.80   7.371    107
       2936.77   7.349     37
       2910.52   7.283    178
       2909.30   7.280    331
       2907.96   7.277    196
       2905.52   7.271     37
       2903.69   7.266    167
       2901.86   7.262    463
       2900.15   7.257    162
       2895.75   7.246    120
       2894.53   7.243    201
       2893.31   7.240    114
       2826.29   7.072    795
       2823.97   7.067    863
       2782.59   6.963    408
       2780.27   6.957    361
       2774.41   6.943    572
       2772.09   6.937    546
       2739.99   6.856   1000
       2731.81   6.836    713
       2729.37   6.830     56
    

in DMSO-d6



KBr disc



nujol mull