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网站主页CAS数据库列表 91-59-8更多图谱2-萘胺(91-59-8)核磁图(13CNMR)

2-萘胺

产品名称 2-萘胺

CAS号91-59-8

分子式C10H9N

分子量143.19

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  • Mass

    MS-NW-8694          
    2-naphthylamine
    C10H9N              (Mass of molecular ion:    143)
    

       Source Temperature: 270 °C
       Sample Temperature: 150 °C
       Reservoir, 75 eV
    

          39.0       1.7
          50.0       1.1
          51.0       1.5
          57.5       1.7
          58.5       3.5
          62.0       1.4
          63.0       3.2
          65.0       1.8
          70.5       4.1
          71.5       7.2
          74.0       1.0
          75.0       1.2
          76.0       1.0
          77.0       1.0
          88.0       1.1
          89.0       3.8
         113.0       1.5
         114.0       2.5
         115.0      33.2
         116.0      17.7
         117.0       2.7
         126.0       2.1
         140.0       1.5
         141.0       1.1
         142.0       4.2
         143.0     100.0
         144.0      11.6
    

400 MHz in CDCl3

90 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C10 H9 N 0.044 g : 0.5 ml CDCl3
    2-naphthylamine
    ChemicalStructure
        Assign.     Shift(ppm)
    A *1 7.674 B 7.627 C *1 7.566 D *2 7.350 E *2 7.210 F 6.925 G 6.892 J 3.76 J(F,G)=2.3HZ. J(B,G)=8.5HZ.

         Hz     ppm     Int.
    

       3077.88   7.702     37
       3071.29   7.685    569
       3070.68   7.684    582
       3067.38   7.676     72
       3063.11   7.665    619
       3062.50   7.663    631
       3057.62   7.651     58
       3052.86   7.639    799
       3049.32   7.630     60
       3044.07   7.617    830
       3035.89   7.597     30
       3035.52   7.596     31
       3028.32   7.578    552
       3027.71   7.576    554
       3020.02   7.557    656
       3019.41   7.556    655
       2948.73   7.379     40
       2945.43   7.371    415
       2944.21   7.367    434
       2941.65   7.361     64
       2938.60   7.353    533
       2937.26   7.350    783
       2935.91   7.347    385
       2930.42   7.333    436
       2929.08   7.330    426
       2892.70   7.239     45
       2889.40   7.230    548
       2888.18   7.227    562
       2882.57   7.213    473
       2881.23   7.210    884
       2880.00   7.207    547
       2877.08   7.200     50
       2874.39   7.193    425
       2781.13   6.959     40
       2780.27   6.957     39
       2778.81   6.954     45
       2775.63   6.946     39
       2768.92   6.929    757
       2766.72   6.923   1000
       2762.21   6.912     76
       2759.40   6.905    987
       2757.08   6.899    648
       2750.85   6.884    866
       2748.54   6.878    671
       1501.10   3.757    187
    


  • 1H NMR 89.56 MHz
    C10 H9 N 0.042 g : 0.5 ml CDCl3
    2-naphthylamine
    ChemicalStructure
        Assign.     Shift(ppm)
    A 7.65 B 7.61 C 7.57 D *1 7.33 E *1 7.21 F 6.91 G 6.86 J 3.68

         Hz     ppm     Int.
    

        691.13   7.717    141
        690.50   7.710    150
        689.38   7.698    124
        689.00   7.694    114
        688.31   7.686    110
        687.00   7.671    192
        686.44   7.665    236
        685.75   7.657    163
        684.56   7.644    161
        683.94   7.637    279
        683.19   7.629    236
        682.63   7.623    213
        681.81   7.613    313
        681.00   7.604    262
        680.44   7.598    194
        679.63   7.589    200
        676.56   7.555    282
        674.94   7.537    154
        673.88   7.525    200
        672.81   7.513    269
        672.19   7.506    250
        665.13   7.427    154
        663.44   7.408    189
        658.44   7.352    363
        656.81   7.334    260
        655.31   7.317     62
        651.19   7.271    464
        649.13   7.248    437
        644.56   7.197    141
        643.44   7.185    231
        642.44   7.174    118
        641.75   7.166    234
        636.81   7.111    113
        635.13   7.092     94
        620.69   6.931     38
        618.63   6.908   1000
        617.06   6.890    266
        616.69   6.886    253
        616.25   6.881    248
        611.13   6.824    340
        608.81   6.798    192
        329.75   3.682    199
    

in CDCl3



CCl4 solution



KBr disc



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