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反式-1,2-二氯环己烷

产品名称 反式-1,2-二氯环己烷

CAS号822-86-6

分子式C6H10Cl2

分子量153.05

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  • Mass

    MS-IW-0074          
    trans-1,2-dichlorocyclohexane
    C6H10Cl2            (Mass of molecular ion:    152)
    

       Source Temperature: 250 °C
       Sample Temperature: 150 °C
       Reservoir, 75 eV
    

          27.0       5.5
          28.0       1.1
          29.0       1.1
          38.0       1.1
          39.0       9.0
          40.0       1.3
          41.0      13.1
          42.0       1.5
          49.0       1.2
          50.0       1.5
          51.0       3.5
          52.0       1.3
          53.0       6.9
          54.0       7.2
          55.0      10.8
          56.0       1.1
          62.0       3.2
          63.0       1.0
          64.0       1.0
          65.0       1.7
          67.0       7.1
          75.0       8.1
          76.0       1.2
          77.0       5.1
          78.0       1.0
          79.0      11.2
          80.0      53.0
          81.0     100.0
          82.0       7.0
          88.0       3.5
          89.0       1.3
          90.0       3.2
         116.0       5.0
         117.0       1.0
         118.0       1.6
         152.0       1.4
    

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C6 H10 Cl2 0.05 ml : 0.5 ml CDCl3
    trans-1,2-dichlorocyclohexane
    ChemicalStructure
        Assign.     Shift(ppm)
    A 4.013 B 2.320 C *1 1.77 D *1 1.73 E 1.419

         Hz     ppm     Int.
    

       1631.10   4.082     34
       1627.20   4.072     42
       1614.62   4.041    221
       1607.54   4.023    836
       1603.88   4.014    843
       1600.59   4.005    795
        954.22   2.388     34
        948.24   2.373     58
        945.43   2.366    103
        941.16   2.355    256
        938.72   2.349    478
        937.62   2.347    411
        936.28   2.343    475
        935.30   2.341    521
        933.96   2.337    499
        932.86   2.335    589
        930.66   2.329    570
        929.32   2.326    438
        928.22   2.323    429
        927.25   2.321    464
        926.03   2.318    459
        924.80   2.315    594
        923.83   2.312    445
        922.61   2.309    521
        921.39   2.306    523
        919.80   2.302    478
        918.95   2.300    484
        916.99   2.295    458
        915.77   2.292    401
        913.33   2.286    265
        732.30   1.833     52
        731.08   1.830     44
        728.64   1.824     65
        727.91   1.822     67
        724.24   1.813    137
        722.17   1.808    205
        720.46   1.803    211
        718.75   1.799    231
        717.53   1.796    351
        716.31   1.793    411
        715.45   1.791    447
        714.23   1.788    597
        712.77   1.784    567
        711.91   1.782    619
        710.94   1.779    488
        708.86   1.774    799
        707.40   1.771    717
        705.20   1.765    945
        701.54   1.756    957
        700.20   1.753    924
        698.85   1.749    895
        697.75   1.746   1000
        694.46   1.738    725
        693.36   1.735    663
        692.14   1.732    544
        690.31   1.728    571
        689.45   1.726    549
        688.48   1.723    557
        687.62   1.721    509
        685.91   1.717    450
        684.94   1.714    474
        684.45   1.713    472
        683.59   1.711    473
        682.37   1.708    403
        680.91   1.704    392
        680.05   1.702    417
        677.73   1.696    287
        676.15   1.692    261
        674.56   1.688    275
        671.14   1.680    175
        667.24   1.670     55
        592.53   1.483     51
        590.21   1.477     55
        585.57   1.466    160
        584.47   1.463    128
        583.13   1.460    144
        582.15   1.457    152
        579.83   1.451    255
        576.17   1.442    479
        574.34   1.438    490
        571.90   1.432    505
        567.38   1.420    652
        566.16   1.417    610
        564.21   1.412    795
        561.04   1.404    491
        557.98   1.397    423
        556.40   1.393    313
        555.30   1.390    267
        552.98   1.384    151
        550.66   1.378    128
        547.97   1.372     82
        546.51   1.368     70
        545.29   1.365     75
    

in CDCl3



liquid film