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网站主页CAS数据库列表 81-65-2更多图谱羟基硝基蒽醌(81-65-2)红外图谱(IR1)

羟基硝基蒽醌

产品名称 羟基硝基蒽醌

CAS号81-65-2

分子式C14H7NO5

分子量269.21

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  • Mass

    MS-IW-3661          
    1-hydroxy-4-nitroanthraquinone
    C14H7NO5            (Mass of molecular ion:    269)
    

       Source Temperature: 140 °C
       Sample Temperature: 100 °C
       Direct, 75 eV
    

          18.0       2.4
          28.0       1.3
          30.0       1.8
          39.0       2.0
          50.0       3.6
          51.0       2.5
          53.0       1.4
          61.0       1.2
          62.0       4.1
          63.0       6.5
          65.0       1.3
          69.0       1.9
          69.5       3.5
          74.0       3.5
          75.0       4.7
          76.0       5.1
          77.0       4.9
          83.0       1.3
          86.0       2.4
          87.0       3.7
          88.0       1.9
          89.0       5.5
          90.0       1.4
          91.0       2.5
          98.0       1.7
          99.0       1.8
         101.0       2.9
         104.0       1.7
         105.0       2.8
         110.0       1.0
         111.0       1.5
         112.0       1.2
         113.0       5.7
         126.0       2.2
         127.0       6.7
         128.0       1.2
         129.0       1.3
         137.0       4.3
         138.0       7.0
         139.0      42.3
         140.0       5.4
         155.0       4.5
         167.0      11.1
         168.0       1.6
         171.0       1.2
         183.0      12.6
         184.0       1.8
         195.0      11.8
         196.0       2.3
         211.0      22.8
         212.0       3.5
         222.0       1.5
         223.0       2.5
         239.0      38.6
         240.0       6.3
         241.0       1.0
         253.0       1.3
         269.0     100.0
         270.0      16.0
         271.0       2.2
    

400 MHz in DMSO-d6


  • 1H NMR 399.65 MHz
    C14 H7 N O5 saturated in DMSO-d6
    1-hydroxy-4-nitroanthraquinone
    ChemicalStructure
        Assign.     Shift(ppm)
    A 8.251 B 8.129 C 8.093 D *1 8.00 E *1 7.98 F 7.546

         Hz     ppm     Int.
    

       3302.49   8.264    395
       3299.93   8.258    305
       3298.95   8.255    277
       3297.24   8.251    271
       3295.04   8.245    328
       3293.46   8.241    503
       3291.50   8.236     62
       3290.65   8.234     62
       3289.67   8.232     90
       3254.03   8.143    379
       3251.95   8.137    271
       3249.63   8.132    282
       3248.29   8.128    311
       3247.80   8.127    294
       3247.44   8.126    299
       3244.87   8.120    503
       3242.80   8.115     68
       3242.43   8.114     68
       3241.82   8.112     79
       3239.14   8.105    915
       3230.10   8.083    989
       3205.93   8.022     68
       3204.96   8.020     79
       3204.59   8.019     85
       3202.51   8.014    181
       3201.29   8.011     79
       3200.93   8.010     79
       3200.44   8.009     90
       3199.71   8.007     90
       3197.27   8.001    605
       3195.43   7.996    859
       3191.89   7.987    960
       3188.60   7.979    701
       3186.65   7.974    418
       3181.15   7.960    119
       3178.96   7.955     79
       3020.26   7.558   1000
       3011.35   7.535    944
    

in DMSO-d6



KBr disc



nujol mull