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网站主页CAS数据库列表 770-71-8更多图谱1-金刚烷甲醇(770-71-8)核磁图(1HNMR)

1-金刚烷甲醇

产品名称 1-金刚烷甲醇

CAS号770-71-8

分子式C11H18O

分子量166.26

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  • Mass

    MS-NW-2585          
    (1-adamantyl)methanol
    C11H18O             (Mass of molecular ion:    166)
    

       Source Temperature: 260 °C
       Sample Temperature: 170 °C
       Reservoir, 75 eV
    

          27.0       1.5
          29.0       1.3
          31.0       1.2
          39.0       2.8
          41.0       4.9
          53.0       1.8
          55.0       3.7
          65.0       1.2
          67.0       6.5
          69.0       1.7
          77.0       3.6
          79.0      16.2
          80.0       1.5
          81.0       5.2
          91.0       3.5
          92.0       1.5
          93.0      15.0
          94.0       1.3
         105.0       1.0
         107.0       5.8
         135.0     100.0
         136.0      11.0
         166.0       3.0
    

90 MHz in CDCl3


  • 1H NMR 89.56 MHz
    C11 H18 O 0.042 g : 0.5 ml CDCl3
    (1-adamantyl)methanol
    ChemicalStructure
        Assign.     Shift(ppm)
    A 3.193 B 1.98 C 1.69 D 1.51 J(B,D)=3.0HZ.

         Hz     ppm     Int.
    

        286.00   3.194   1000
        178.31   1.991    204
        176.19   1.968    193
        164.56   1.838     37
        154.06   1.721    456
        151.94   1.697    836
        143.31   1.601     38
        141.50   1.580     52
        141.13   1.576     54
        136.75   1.527    812
        133.75   1.494    727
    

in CDCl3



CCl4 solution



KBr disc



nujol mull



4880 A,200 M,powder