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网站主页CAS数据库列表 764-35-2更多图谱2-已炔(764-35-2)核磁图(13CNMR)

2-已炔

产品名称 2-已炔

CAS号764-35-2

分子式C6H10

分子量82.14

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  • Mass

    MS-NW-5113          
    2-hexyne
    C6H10               (Mass of molecular ion:     82)
    

       Source Temperature: 260 °C
       Sample Temperature: 190 °C
       Reservoir, 75 eV
    

          26.0       3.6
          27.0      29.4
          28.0       5.0
          29.0       9.3
          37.0       2.3
          38.0       3.6
          39.0      35.8
          40.0       6.2
          41.0      45.5
          42.0      12.2
          43.0       4.1
          49.0       1.1
          50.0       8.4
          51.0      13.2
          52.0      11.8
          53.0      60.6
          54.0      37.8
          55.0       6.7
          56.0       1.3
          57.0       1.3
          62.0       1.5
          63.0       2.7
          65.0       9.4
          66.0       4.0
          67.0     100.0
          68.0       6.0
          74.0       1.3
          77.0       4.1
          78.0       2.0
          79.0       7.2
          80.0       2.6
          81.0      12.7
          82.0      74.1
          83.0       5.1
    

400 MHz in CDCl3

90 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C6 H10 0.04 ml : 0.5 ml CDCl3
    2-hexyne
    ChemicalStructure
        Assign.     Shift(ppm)
    A 2.097 B 1.781 C 1.495 D 0.967

         Hz     ppm     Int.
    

        849.37   2.126     40
        846.80   2.119    123
        844.24   2.113    137
        842.16   2.108    104
        839.72   2.102    247
        837.16   2.095    255
        834.59   2.089    112
        832.64   2.084    147
        830.08   2.078    139
        827.51   2.071     51
        714.23   1.788    646
        711.67   1.781   1000
        709.11   1.775    614
        615.97   1.542     47
        608.52   1.523    158
        601.44   1.505    306
        594.12   1.487    308
        586.91   1.469    188
        579.71   1.451     49
        393.43   0.985    461
        389.04   0.974     31
        386.23   0.967    794
        378.66   0.948    390
    


  • 1H NMR 89.56 MHz
    C6 H10 0.04 ml : 0.5 ml CDCl3
    2-hexyne
    ChemicalStructure
        Assign.     Shift(ppm)
    A 2.083 B 1.778 C 1.50 D 0.97 J(A,B)=2.5HZ

         Hz     ppm     Int.
    

        197.00   2.200     40
        195.81   2.187     48
        194.38   2.171     53
        193.31   2.159     62
        191.69   2.141     66
        189.06   2.111    138
        187.31   2.092    114
        186.50   2.083    159
        185.13   2.068     95
        184.06   2.056     84
        182.81   2.042    104
        180.50   2.016    104
        179.63   2.006     91
        178.38   1.992     54
        177.13   1.978     52
        161.69   1.806    577
        159.19   1.778   1000
        156.63   1.749    429
        154.19   1.722     58
        152.13   1.699     54
        151.69   1.694     57
        149.06   1.665     36
        146.44   1.636     45
        145.63   1.627     67
        144.25   1.611    116
        138.13   1.543    102
        137.50   1.536    170
        136.44   1.524    118
        134.69   1.504     34
        134.38   1.501     33
        134.25   1.499     33
        133.56   1.492     39
        131.25   1.466    102
        130.69   1.460    131
        129.63   1.448    157
        126.25   1.410     35
        124.56   1.391     61
        123.25   1.377    115
        117.06   1.308     39
        116.44   1.301     40
         93.94   1.049    194
         93.06   1.040    300
         90.06   1.006     42
         89.44   0.999     45
         88.63   0.990     49
         86.50   0.966    658
         85.81   0.959    300
         82.63   0.923     49
         81.88   0.915     42
         81.19   0.907     41
         79.88   0.892    117
         78.81   0.880    173
         77.38   0.865     88
    

in CDCl3



liquid film