图谱信息 供应商 相关产品
网站主页CAS数据库列表 75-77-4更多图谱三甲基氯硅烷(75-77-4)质谱(MS)

三甲基氯硅烷

产品名称 三甲基氯硅烷

CAS号75-77-4

分子式C3H9ClSi

分子量108.64

展开


  • Mass

    MS-NW-3310          
    chlorotrimethylsilane
    C3H9ClSi            (Mass of molecular ion:    108)
    

       Source Temperature: 280 °C
       Sample Temperature: 180 °C
       Reservoir, 75 eV
    

          28.0       1.4
          29.0       2.1
          42.0       2.1
          43.0       6.7
          44.0       2.0
          45.0       4.8
          53.0       1.6
          55.0       1.0
          63.0      10.2
          64.0       1.4
          65.0      12.2
          67.0       3.6
          72.0       2.6
          73.0      35.2
          74.0       3.0
          75.0       1.6
          77.0       1.3
          78.0       1.4
          79.0       2.5
          92.0       1.0
          93.0     100.0
          94.0       7.8
          95.0      35.4
          96.0       2.5
          97.0       1.2
         108.0       3.6
         110.0       1.2
         147.0       2.1
    

parameter in CCl4

90 MHz in CDCl3


  • 1H NMR 300 MHz
    C3 H9 Cl Si 5 vol% in CCl4
    chlorotrimethylsilane
    ChemicalStructure
        Parameter     ppm  Hz
    D(A) 0.42 SCHMIDBAUR,H. J.AM.CHEM.SOC. 85, 2336 (1963) J(C-13,A):120.5HZ. J(SI-29,A):7.10HZ.

         Hz     ppm     Int.
    

        126.00   0.420   1000
    


  • 1H NMR 89.56 MHz
    C3 H9 Cl Si 0.04 ml : 0.5 ml CDCl3
    chlorotrimethylsilane
    ChemicalStructure
        Assign.     Shift(ppm)
    A 0.431 J(SI-29,A)=7.0HZ.

         Hz     ppm     Int.
    

         42.13   0.471     45
         38.63   0.432   1000
         35.13   0.393     48
    

in CDCl3



liquid film