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3,5-二硝基苄氯

产品名称 3,5-二硝基苄氯

CAS号74367-78-5

分子式C7H5ClN2O4

分子量216.58

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  • Mass

    MS-NW-7259          
    3,5-dinitrobenzyl chloride
    C7H5ClN2O4          (Mass of molecular ion:    216)
    

       Source Temperature: 140 °C
       Sample Temperature: 120 °C
       Direct, 75 eV
    

          28.0       2.1
          30.0      24.5
          37.0       1.5
          38.0       3.2
          39.0      12.3
          46.0       1.0
          49.0       1.7
          50.0       4.8
          51.0       7.7
          52.0       1.6
          61.0       2.4
          62.0      10.5
          63.0      26.9
          64.0       2.5
          65.0       1.5
          73.0       4.5
          74.0       2.6
          75.0      10.0
          76.0       2.4
          77.0       8.3
          78.0       1.1
          85.0       1.7
          86.0       3.1
          87.0       4.6
          88.0       4.2
          89.0      32.0
          90.0       2.8
          97.0       1.2
         105.0      11.2
         106.0       1.1
         112.0       1.3
         123.0      27.0
         124.0      17.3
         125.0      10.2
         126.0       6.0
         134.0       1.0
         135.0       6.5
         140.0       6.4
         142.0       2.2
         169.0       2.5
         170.0      12.6
         171.0       1.8
         172.0       4.2
         181.0     100.0
         182.0       8.8
         183.0       1.2
         199.0       4.4
         200.0       1.2
         201.0       1.6
         216.0      47.1
         217.0       4.3
         218.0      16.1
         219.0       1.4
    

90 MHz in CDCl3


  • 1H NMR 89.56 MHz
    C7 H5 Cl N2 O4 0.042 g : 0.5 ml CDCl3
    3,5-dinitrobenzyl chloride
    ChemicalStructure
        Assign.     Shift(ppm)
    A 9.003 B 8.622 C 4.785 J(A,B)=2.1HZ J(B,C)=1.0HZ

         Hz     ppm     Int.
    

        810.88   9.055     27
        810.50   9.050     30
        808.50   9.028    166
        806.44   9.005    310
        804.38   8.982    186
        802.56   8.962     27
        777.31   8.680     36
        773.06   8.632    672
        771.00   8.609    584
        428.81   4.788   1000
        428.38   4.784    932
    

in CDCl3



KBr disc



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