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网站主页CAS数据库列表 73579-08-5更多图谱1-甲基-4-(甲氨基)哌啶(73579-08-5)核磁图(1HNMR)

1-甲基-4-(甲氨基)哌啶

产品名称 1-甲基-4-(甲氨基)哌啶

CAS号73579-08-5

分子式C7H16N2

分子量128.22


  • Mass

    MS-NW-9662          
    N(4),1-dimethyl-4-piperidinamine
    C7H16N2             (Mass of molecular ion:    128)
    

       Source Temperature: 270 °C
       Sample Temperature: 150 °C
       Reservoir, 75 eV
    

          15.0       3.0
          18.0       1.5
          27.0       4.1
          28.0       7.6
          29.0       4.2
          30.0       6.0
          39.0       3.4
          41.0       6.5
          42.0      38.4
          43.0      59.1
          44.0      29.9
          45.0       1.0
          52.0       1.0
          53.0       2.0
          54.0       4.4
          55.0      13.2
          56.0      14.3
          57.0      12.7
          58.0      11.2
          67.0       1.2
          68.0       8.6
          69.0       4.4
          70.0      34.3
          71.0      17.7
          72.0       2.2
          79.0       1.1
          80.0       1.0
          81.0       1.8
          82.0      27.3
          83.0       2.3
          84.0       6.5
          85.0       3.4
          94.0       2.6
          96.0      64.1
          97.0     100.0
          98.0      12.8
          99.0       3.7
         128.0       4.5
         129.0       1.3
    

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C7 H16 N2 0.05 ml : 0.5 ml CDCl3
    N(4),1-dimethyl-4-piperidinamine
    ChemicalStructure
        Assign.     Shift(ppm)
    A 2.805 B 2.427 C 2.329 D 2.263 E 1.987 F 1.873 G 1.379 J 1.23 ASSIGNED BY H-H COSY.

         Hz     ppm     Int.
    

       1127.20   2.821     83
       1118.16   2.798     61
       1115.11   2.791     90
        969.97   2.428   1000
        942.14   2.358     35
        935.79   2.342     40
        931.76   2.332     68
        927.73   2.322     44
        925.54   2.316     32
        921.39   2.306     38
        908.45   2.274     68
        904.42   2.264    950
        807.13   2.020     55
        804.81   2.014     63
        795.41   1.991    102
        793.21   1.985    116
        783.81   1.962     56
        781.62   1.956     64
        757.69   1.896     67
        756.84   1.894     72
        755.49   1.891     77
        754.15   1.888     73
        752.93   1.884     71
        749.02   1.875     49
        745.12   1.865     75
        744.02   1.862     81
        742.55   1.859     86
        741.33   1.855     80
        740.36   1.853     77
        569.82   1.426     39
        566.04   1.417     40
        558.35   1.398     67
        557.01   1.394     72
        555.66   1.391     71
        554.57   1.388     75
        546.63   1.368     67
        545.65   1.366     65
        544.19   1.362     66
        542.72   1.358     63
        535.03   1.339     30
        531.25   1.330     30
    

in CDCl3



liquid film