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2-甲基-5-叔丁基噻吩

产品名称 2-甲基-5-叔丁基噻吩

CAS号7340-90-1

分子式C11H16S

分子量180.31

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  • Mass

    MS-IW-7191          
    5-tert-butyl-2-methylbenzenethiol
    C11H16S             (Mass of molecular ion:    180)
    

       Source Temperature: 220 °C
       Sample Temperature: 150 °C
       Reservoir, 75 eV
    

          27.0       1.0
          29.0       1.2
          39.0       3.0
          41.0       5.2
          45.0       3.9
          51.0       2.0
          53.0       1.3
          55.0       1.0
          57.0       1.9
          63.0       1.6
          64.0       1.1
          65.0       2.2
          68.5       1.2
          69.0       1.0
          73.0       7.3
          74.0       1.1
          75.0       1.1
          77.0       3.6
          78.0       1.1
          79.0       1.4
          81.5       1.0
          82.5       2.2
          89.0       1.4
          91.0       8.5
          92.0       1.8
         103.0       1.3
         105.0       2.6
         115.0       5.5
         116.0       3.5
         117.0       3.7
         121.0       1.0
         123.0       4.2
         124.0       1.6
         125.0       8.6
         127.0       1.0
         128.0       1.7
         129.0       1.8
         130.0       1.2
         131.0       6.6
         132.0       6.0
         133.0       1.0
         134.0       1.8
         135.0       1.2
         137.0      13.4
         138.0       1.6
         147.0       1.4
         149.0       3.3
         150.0       1.2
         163.0       1.8
         164.0       2.5
         165.0     100.0
         166.0      11.8
         167.0       5.0
         179.0       3.1
         180.0      39.9
         181.0       5.3
         182.0       2.1
    

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C11 H16 S 0.05 ml : 0.5 ml CDCl3
    5-tert-butyl-2-methylbenzenethiol
    ChemicalStructure
        Assign.     Shift(ppm)
    A 7.281 B 7.09 C 7.07 D 3.25 E 2.280 F 1.275 CONFIRMED BY LAOCN PROGRAM

         Hz     ppm     Int.
    

       2911.62   7.286     86
       2909.91   7.282     93
       2864.99   7.169     44
       2839.36   7.105     25
       2837.52   7.101     21
       2831.42   7.085    117
       2829.59   7.081    124
       2827.03   7.074    126
       2819.09   7.054     25
       1299.93   3.253    174
        911.13   2.280    412
        516.48   1.293     32
        509.52   1.275   1000
    

in CDCl3



liquid film