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MassMS2014-05075CW 4-aminomethyl-2-methoxyphenol hydrochloride C8H11NO2 HCl (Mass of molecular ion: 153)
Source Temperature: 245 °C Sample Temperature: 20 °C Direct, 70 eV
15.0 1.5 27.0 2.3 28.0 7.2 29.0 1.7 30.0 12.5 35.0 3.3 36.0 18.4 37.0 1.1 38.0 6.2 39.0 8.4 40.0 1.5 41.0 2.4 42.0 1.0 43.0 1.1 50.0 4.2 51.0 9.6 52.0 8.5 53.0 5.8 54.0 3.7 55.0 3.8 62.0 2.3 63.0 5.0 64.0 2.8 65.0 20.0 66.0 5.7 67.0 6.1 68.0 1.0 76.0 1.2 77.0 8.6 78.0 4.1 79.0 4.2 80.0 10.0 81.0 10.0 82.0 8.6 83.0 2.5 90.0 1.6 91.0 1.8 92.0 5.0 93.0 24.8 94.0 12.0 95.0 6.2 105.0 5.6 106.0 5.4 107.0 12.7 108.0 7.2 109.0 24.3 110.0 31.4 111.0 3.8 118.0 2.0 119.0 1.1 120.0 3.9 121.0 9.4 122.0 62.9 123.0 6.5 124.0 5.3 125.0 12.9 126.0 1.0 134.0 2.2 135.0 9.5 136.0 74.5 137.0 77.2 138.0 13.8 139.0 1.2 150.0 3.0 151.0 1.1 152.0 97.8 153.0 100.0 154.0 9.0
400 MHz in DMSO-d6
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1H NMR 399.65 MHz C8 H11 N O2 0.036 g : 0.5 ml DMSO-d6 4-aminomethyl-2-methoxyphenol hydrochloride 
Assign. Shift(ppm)
A 9.26 B 8.51 C 7.223 D 6.874 E 6.823 F 3.878 G 3.777
Hz ppm Int.3702.39 9.265 26 3399.35 8.506 88 2887.88 7.227 161 2886.05 7.222 163 2753.45 6.890 61 2751.62 6.886 58 2745.51 6.870 114 2743.53 6.865 115 2729.80 6.831 242 2721.71 6.811 132 1552.73 3.886 105 1547.39 3.872 105 1509.55 3.778 1000
in DMSO-d6
KBr disc
nujol mull
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