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亞甲去甲[0XA29C]

产品名称 亞甲去甲[0XA29C]

CAS号694-91-7

分子式C8H10

分子量106.17

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  • Mass

    MS-NW-8866          
    5-methylene-2-norbornene
    C8H10               (Mass of molecular ion:    106)
    

       Source Temperature: 260 °C
       Sample Temperature: 150 °C
       Reservoir, 75 eV
    

          27.0       8.3
          38.0       2.6
          39.0      21.1
          40.0       6.7
          41.0       5.1
          50.0       4.6
          51.0      11.6
          52.0       5.4
          53.0       4.1
          62.0       1.6
          63.0       4.5
          64.0       1.0
          65.0      14.1
          66.0     100.0
          67.0       7.6
          74.0       1.0
          77.0      16.3
          78.0      44.3
          79.0      17.6
          80.0       3.2
          89.0       1.1
          91.0      77.7
          92.0       6.6
          93.0       1.2
         103.0       4.6
         104.0       1.3
         105.0      18.4
         106.0      31.5
         107.0       2.9
    

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C8 H10 0.05 ml : 0.5 ml CDCl3
    5-methylene-2-norbornene
    ChemicalStructure
        Assign.     Shift(ppm)
    A *1 6.108 B *1 6.060 C *2 4.979 D *2 4.705 E 3.139 F 2.949 G *3 2.244 J *3 1.746 K *4 1.587 L *4 1.410

         Hz     ppm     Int.
    

       2446.17   6.121    518
       2443.24   6.114    532
       2440.55   6.107    827
       2437.62   6.100    842
       2425.90   6.071    647
       2425.17   6.069    667
       2422.85   6.063    632
       2422.12   6.061    649
       2421.26   6.059    412
       2420.29   6.057    412
       2419.68   6.055    388
       2417.24   6.049    387
       2416.50   6.047    374
       1989.87   4.980    904
       1881.23   4.708   1000
       1880.74   4.706    938
       1879.88   4.704    935
       1879.52   4.703   1000
       1256.59   3.145    586
       1255.49   3.142    683
       1255.00   3.141    688
       1254.39   3.139    689
       1254.03   3.138    681
       1252.93   3.136    584
       1179.93   2.953    570
       1179.44   2.952    575
       1178.96   2.950    576
       1178.47   2.949    574
        903.93   2.262    362
        903.32   2.261    323
        902.22   2.258    419
        900.51   2.254    358
        889.77   2.227    329
        889.28   2.226    413
        888.67   2.224    367
        888.18   2.223    348
        887.45   2.221    488
        886.72   2.219    345
        886.23   2.218    348
        885.74   2.217    402
        706.67   1.769    380
        706.30   1.768    384
        705.20   1.765    381
        703.49   1.761    398
        691.65   1.731    329
        690.43   1.728    326
        688.84   1.724    345
        640.26   1.603    389
        638.67   1.599    388
        637.08   1.595    363
        632.08   1.582    470
        630.49   1.578    473
        628.91   1.574    438
        567.38   1.420    729
        559.20   1.400    600
    

in CDCl3



liquid film



4880 A,150M,liquid