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N-丁基乙基硫醚

产品名称 N-丁基乙基硫醚

CAS号638-46-0

分子式C6H14S

分子量118.24

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  • Mass

    MS-NW-1480          
    butyl ethyl sulfide
    C6H14S              (Mass of molecular ion:    118)
    

       Source Temperature: 260 °C
       Sample Temperature: 180 °C
       Reservoir, 75 eV
    

          15.0       1.0
          18.0       1.0
          26.0       3.3
          27.0      35.6
          28.0       9.4
          29.0      49.5
          30.0       1.2
          34.0       1.2
          35.0       9.2
          39.0      10.9
          40.0       2.0
          41.0      49.1
          42.0       3.6
          43.0       4.3
          45.0      11.8
          46.0      11.8
          47.0      47.9
          48.0       6.4
          49.0       2.4
          53.0       1.9
          54.0       1.0
          55.0      16.9
          56.0      68.2
          57.0      17.1
          58.0       3.1
          59.0       5.7
          60.0       6.1
          61.0      37.5
          62.0      47.0
          63.0      19.6
          64.0       2.4
          66.0       1.4
          75.0     100.0
          76.0       8.3
          77.0       4.8
          89.0      24.6
          90.0       2.8
          91.0       1.3
          94.0       1.0
         103.0       1.9
         118.0      56.4
         119.0       4.4
         120.0       2.7
         122.0       1.5
    

400 MHz in CDCl3

90 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C6 H14 S 0.05 ml : 0.5 ml CDCl3
    butyl ethyl sulfide
    ChemicalStructure
        Assign.     Shift(ppm)
    A 2.530 B 2.527 C 1.569 D 1.416 E 1.255 F 0.922

         Hz     ppm     Int.
    

       1023.56   2.562    147
       1016.11   2.543    522
       1008.79   2.525    568
       1001.10   2.505    287
        642.70   1.609     50
        642.09   1.607     45
        636.11   1.592     97
        635.50   1.591    114
        634.16   1.587     62
        632.93   1.584     66
        629.03   1.574     82
        628.17   1.572    159
        625.12   1.565     66
        621.09   1.555    120
        620.24   1.552    116
        618.53   1.548     58
        618.04   1.547     55
        613.04   1.534     68
        612.43   1.533     63
        583.13   1.460     47
        576.05   1.442    114
        570.68   1.428     51
        570.07   1.427     55
        568.85   1.424    135
        568.12   1.422    135
        563.35   1.410     51
        562.74   1.409     53
        561.52   1.406    104
        560.42   1.403    137
        553.34   1.385     83
        546.26   1.367     31
        508.42   1.273    569
        505.62   1.266     31
        501.10   1.254   1000
        493.53   1.235    514
        375.24   0.939    446
        372.07   0.931     35
        367.92   0.921    829
        365.48   0.915     33
        360.60   0.903    354
    


  • 1H NMR 89.56 MHz
    C6 H14 S 0.04 ml : 0.5 ml CDCl3
    butyl ethyl sulfide
    ChemicalStructure
        Assign.     Shift(ppm)
    A 2.53 B 2.52 C 1.57 D 1.44 E 1.26 F 0.92

         Hz     ppm     Int.
    

        238.56   2.664     78
        232.94   2.601     88
        230.75   2.577    253
        228.44   2.551     88
        226.19   2.526    182
        223.38   2.495    273
        219.25   2.449    128
        216.44   2.417     95
        148.75   1.661     58
        146.56   1.637     64
        142.63   1.593     75
        141.63   1.582     84
        140.50   1.569     77
        139.25   1.555    129
        135.88   1.518    156
        134.31   1.500    153
        131.88   1.473    179
        129.25   1.444    125
        127.69   1.426    102
        126.81   1.416     61
        125.13   1.398     70
        124.56   1.391     58
        123.50   1.379     55
        123.06   1.375     55
        122.63   1.370     58
        122.06   1.363     56
        121.13   1.353     60
        119.44   1.334    477
        118.38   1.322    110
        116.06   1.296     52
        115.25   1.287     55
        114.69   1.281     51
        113.81   1.271     30
        112.31   1.255   1000
        109.63   1.225     40
        109.31   1.221     40
        104.69   1.169    335
         88.88   0.993    196
         88.13   0.985    167
         85.69   0.957     55
         84.19   0.941     54
         82.31   0.920    483
         79.88   0.892    129
         77.69   0.868     47
         77.13   0.862     46
         76.06   0.850     71
         74.94   0.837     89
         73.13   0.817     52
    

in CDCl3



CCl4 solution



liquid film