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4-甲基苯肼盐酸盐

产品名称 4-甲基苯肼盐酸盐

CAS号637-60-5

分子式C7H11ClN2

分子量158.63

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  • Mass

    MS-NW-0632          
    p-tolylhydrazine hydrochloride
    C7H10N2 HCl         (Mass of molecular ion:    122)
    

       Source Temperature: 200 °C
       Sample Temperature: 160 °C
       Direct, 75 eV
    

          17.0       1.3
          18.0       5.2
          26.0       1.2
          27.0       5.3
          28.0       4.2
          29.0       3.2
          31.0       1.6
          35.0       5.7
          36.0      32.8
          37.0       1.9
          38.0      10.4
          39.0      12.0
          40.0       1.5
          41.0       3.4
          43.0       1.2
          50.0       6.1
          51.0      12.5
          52.0       8.1
          53.0       5.1
          54.0       1.1
          61.0       1.2
          62.0       2.6
          63.0       6.3
          64.0       2.3
          65.0      12.7
          66.0       1.8
          67.0       1.2
          74.0       1.0
          75.0       1.0
          76.0       1.6
          77.0      36.1
          78.0      16.6
          79.0      40.0
          80.0       3.6
          89.0       3.1
          90.0       1.8
          91.0      24.5
          92.0       9.4
          93.0       3.5
          94.0       1.6
         104.0       8.9
         105.0       7.1
         106.0      56.9
         107.0      12.5
         120.0       2.1
         121.0       9.4
         122.0     100.0
         123.0       8.5
    

90 MHz in D2O


  • 1H NMR 89.56 MHz
    C7 H10 N2 0.043 g : 0.5 ml D2O
    p-tolylhydrazine hydrochloride
    ChemicalStructure
        Assign.     Shift(ppm)
    A 7.26 B 7.04 C 4.83 D 2.311 C-PEAK INCLUDES H2O.

         Hz     ppm     Int.
    

        656.19   7.327     75
        655.81   7.323     76
        647.56   7.231    159
        635.50   7.096     49
        633.25   7.071    202
        631.06   7.047     57
        626.69   6.998     47
        624.63   6.975     93
        432.31   4.828   1000
        207.00   2.312    444
    

in D2O



KBr disc



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