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网站主页CAS数据库列表 6361-21-3更多图谱2-氯-5-硝基苯甲醛(6361-21-3)红外图谱(IR2)

2-氯-5-硝基苯甲醛

产品名称 2-氯-5-硝基苯甲醛

CAS号6361-21-3

分子式C7H4ClNO3

分子量185.56

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  • Mass

    MS-NW-3550          
    2-chloro-5-nitrobenzaldehyde
    C7H4ClNO3           (Mass of molecular ion:    185)
    

       Source Temperature: 280 °C
       Sample Temperature: 180 °C
       Reservoir, 75 eV
    

          28.0       3.9
          29.0       6.5
          30.0       9.5
          36.0       1.4
          37.0       4.5
          38.0       3.3
          39.0       1.7
          49.0       2.6
          50.0      16.8
          51.0       7.7
          53.0       1.1
          61.0       3.7
          62.0       3.3
          63.0       5.5
          64.0       1.1
          72.0       1.0
          73.0       6.5
          74.0      23.6
          75.0     100.0
          76.0      11.5
          84.0       3.6
          85.0       6.2
          86.0       1.9
          87.0       2.5
          99.0      10.4
         101.0       3.8
         103.0       4.2
         109.0       2.1
         110.0      11.5
         111.0      25.2
         112.0       5.4
         113.0       8.4
         126.0       2.2
         127.0       2.0
         138.0      15.7
         139.0      23.6
         140.0       7.0
         141.0       7.9
         149.0       1.3
         155.0       5.2
         157.0       2.1
         169.0       1.8
         184.0      75.1
         185.0      75.9
         186.0      30.8
         187.0      25.9
         188.0       2.4
    

90 MHz in CDCl3


  • 1H NMR 89.56 MHz
    C7 H4 Cl N O3 0.043 g : 0.5 ml CDCl3
    2-chloro-5-nitrobenzaldehyde
    ChemicalStructure
        Assign.     Shift(ppm)
    A 10.497 B 8.736 C 8.387 D 7.709 J(B,C)=2.8HZ. J(C,D)=8.8HZ.

         Hz     ppm     Int.
    

        940.21  10.499   1000
        784.20   8.757    263
        781.35   8.725    312
        757.62   8.460    204
        754.83   8.429    166
        748.83   8.362    260
        746.04   8.331    229
        694.34   7.753    351
        685.55   7.655    270
    

in CDCl3



KBr disc



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