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网站主页CAS数据库列表 6336-72-7更多图谱2-氯-3-吗啉-1,4-萘醌(6336-72-7)核磁图(1HNMR)

2-氯-3-吗啉-1,4-萘醌

产品名称 2-氯-3-吗啉-1,4-萘醌

CAS号6336-72-7

分子式C14H12ClNO3

分子量277.7


  • Mass

    MS-NW-7905          
    2-chloro-3-morpholino-1,4-naphthoquinone
    C14H12ClNO3         (Mass of molecular ion:    277)
    

       Source Temperature: 180 °C
       Sample Temperature: 130 °C
       Direct, 75 eV
    

          15.0       2.6
          18.0       4.0
          26.0       1.8
          27.0       7.1
          28.0       9.1
          29.0       3.1
          30.0       2.0
          31.0       2.0
          36.0       1.8
          38.0       1.0
          39.0       4.2
          41.0       2.8
          42.0      17.1
          43.0       2.9
          44.0       1.2
          45.0       6.6
          50.0       9.7
          51.0       6.0
          52.0       3.9
          53.0       1.7
          54.0       2.5
          55.0       3.0
          56.0      10.6
          57.0       3.4
          58.0       1.2
          59.0       1.0
          61.0       1.0
          62.0       2.2
          63.0       2.7
          64.0       2.1
          66.0       1.4
          68.0       2.3
          69.0       1.0
          70.0       1.5
          72.0       7.6
          73.0       1.3
          74.0       6.4
          75.0      10.6
          76.0      19.2
          77.0       8.2
          77.5       1.1
          78.0       1.8
          80.0       2.8
          85.0       1.6
          86.0       5.1
          87.0       6.4
          88.0       3.0
          89.0       3.2
          94.0       1.2
          95.5       1.9
          98.0       1.4
          99.0       8.5
         100.0       3.5
         101.0      13.8
         102.0       5.1
         103.0       1.6
         104.0       7.0
         105.0       6.2
         109.0       1.7
         109.5       2.9
         110.0       1.0
         110.5       1.1
         111.0       1.5
         113.0       1.6
         114.0       5.7
         115.0       3.6
         116.0       1.3
         116.5       1.3
         123.0       2.3
         123.5       5.2
         124.0       1.3
         124.5       1.8
         125.0       1.1
         126.0       5.2
         127.0       3.6
         128.0       6.1
         129.0      20.4
         130.0       4.3
         135.0       8.4
         136.0       4.3
         137.0       3.4
         138.0       1.8
         140.0       1.0
         143.0       1.9
         149.0       1.4
         151.0       1.1
         154.0      12.4
         155.0       2.7
         156.0       4.0
         157.0      81.5
         158.0      10.5
         159.0       1.9
         163.0       6.0
         164.0       2.3
         165.0       2.8
         166.0       1.0
         167.0       1.1
         171.0       4.2
         172.0       3.7
         173.0       1.6
         177.0       2.2
         179.0       1.0
         182.0       1.0
         183.0       2.8
         184.0       5.3
         185.0       3.7
         186.0       3.7
         191.0       4.8
         192.0      16.8
         193.0       4.8
         194.0       6.2
         195.0       1.5
         196.0       1.1
         198.0       7.0
         199.0       2.0
         200.0       1.1
         205.0       2.2
         206.0      17.1
         207.0       6.8
         208.0       6.6
         209.0       2.7
         210.0       2.8
         211.0       3.5
         212.0       9.1
         213.0       3.6
         214.0       4.5
         216.0       1.5
         218.0       6.8
         219.0       9.0
         220.0      97.1
         221.0      15.7
         222.0      32.6
         223.0       5.0
         224.0       5.7
         225.0       1.1
         226.0       1.1
         233.0      12.8
         234.0       8.4
         235.0       5.5
         236.0       2.8
         241.0       3.4
         242.0      32.8
         243.0       6.3
         244.0       1.1
         246.0      17.0
         247.0       2.9
         248.0       6.8
         249.0       1.3
         276.0       1.9
         277.0     100.0
         278.0      16.9
         279.0      35.0
         280.0       5.7
         281.0       1.1
    

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C14 H12 Cl N O3 0.040 g : 0.5 ml CDCl3
    2-chloro-3-morpholino-1,4-naphthoquinone
    ChemicalStructure
        Assign.     Shift(ppm)
    A 8.096 B 7.997 C *1 7.71 D *1 7.67 E 3.870 F 3.630

         Hz     ppm     Int.
    

       3240.48   8.109    265
       3239.01   8.105    333
       3233.76   8.092    239
       3232.91   8.090    269
       3231.81   8.087    293
       3231.45   8.086    280
       3200.68   8.009    251
       3200.32   8.008    258
       3199.10   8.005    243
       3198.36   8.003    224
       3193.12   7.990    358
       3191.65   7.987    297
       3088.99   7.730    115
       3087.40   7.726    144
       3085.33   7.721     36
       3081.54   7.711    329
       3079.96   7.707    348
       3074.34   7.693    340
       3072.75   7.689    431
       3071.04   7.685    348
       3065.43   7.671    344
       3063.84   7.667    306
       3060.42   7.658     33
       3057.98   7.652    126
       3056.52   7.648    105
       1551.51   3.883    822
       1547.00   3.871   1000
       1542.24   3.859    952
       1532.96   3.836     35
       1532.59   3.835     35
       1464.72   3.666     38
       1455.08   3.641    962
       1450.32   3.629    990
       1445.80   3.618    793
       1436.16   3.594     32
    

in CDCl3



KBr disc



nujol mull