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网站主页CAS数据库列表 629-03-8更多图谱1,6-二溴己烷(629-03-8)质谱(MS)

1,6-二溴己烷

产品名称 1,6-二溴己烷

CAS号629-03-8

分子式C6H12Br2

分子量243.97

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  • Mass

    MS-NW-1301          
    1,6-dibromohexane
    C6H12Br2            (Mass of molecular ion:    242)
    

       Source Temperature: 260 °C
       Sample Temperature: 180 °C
       Reservoir, 75 eV
    

          26.0       1.4
          27.0      17.6
          28.0       2.3
          29.0      10.7
          39.0      11.0
          40.0       2.9
          41.0      40.2
          42.0       6.4
          43.0      19.3
          53.0       3.2
          54.0       2.7
          55.0      65.1
          56.0       5.6
          57.0       4.7
          67.0       4.5
          69.0       4.5
          81.0       1.8
          82.0       5.8
          83.0     100.0
          84.0       6.6
          93.0       1.3
          95.0       1.2
         107.0       4.7
         109.0       4.4
         121.0       3.7
         123.0       3.3
         135.0       1.9
         137.0       1.9
         162.0       4.1
         163.0       6.4
         164.0       4.3
         165.0       6.2
    

90 MHz in CDCl3


  • 1H NMR 89.56 MHz
    C6 H12 Br2 0.04 ml : 0.5 ml CDCl3
    1,6-dibromohexane
    ChemicalStructure
        Assign.     Shift(ppm)
    A 3.409 B 1.88 C 1.50

         Hz     ppm     Int.
    

        312.63   3.491    392
        306.00   3.417   1000
        299.44   3.344    602
        181.94   2.032     39
        180.88   2.020     38
        180.31   2.014     37
        179.44   2.004     39
        176.94   1.976     66
        175.00   1.954    135
        174.06   1.944    123
        170.75   1.907    114
        168.75   1.885    188
        167.81   1.874    193
        164.69   1.839    112
        162.06   1.810    170
        158.69   1.772     74
        157.88   1.763     69
        157.06   1.754     71
        156.38   1.747     67
        155.38   1.735     82
        153.25   1.712     37
        152.25   1.700     40
        150.50   1.681     37
        149.63   1.671     36
        149.13   1.666     39
        145.69   1.627     50
        143.88   1.607     48
        143.50   1.603     47
        140.44   1.569    129
        138.31   1.545    201
        135.50   1.513    192
        135.00   1.508    195
        134.56   1.503    196
        133.94   1.496    199
        131.44   1.468    268
        128.69   1.437    130
        127.38   1.423    178
        125.00   1.396     70
        123.81   1.383     86
    

in CDCl3



CCl4 solution



liquid film