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3,5-二氯苯胺

产品名称 3,5-二氯苯胺

CAS号626-43-7

分子式C6H5Cl2N

分子量162.02

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  • Mass

    MS-NW-1615          
    3,5-dichloroaniline
    C6H5Cl2N            (Mass of molecular ion:    161)
    

       Source Temperature: 240 °C
       Sample Temperature: 180 °C
       Reservoir, 75 eV
    

          28.0       2.7
          37.0       2.5
          38.0       3.0
          39.0       3.0
          41.0       2.8
          44.5       4.2
          45.5       1.3
          49.0       1.0
          50.0       1.4
          52.0       3.6
          61.0       3.4
          62.0       5.9
          62.5       4.9
          63.0      13.4
          63.5       1.5
          64.0       3.2
          65.0       2.2
          73.0       4.6
          74.0       1.7
          75.0       1.7
          80.5       4.5
          81.5       2.9
          88.0       1.0
          89.0       2.2
          90.0      17.1
          91.0       4.5
          97.0       1.4
          98.0       2.3
          99.0      14.8
         100.0       1.7
         101.0       5.1
         124.0       1.0
         125.0       6.5
         126.0      12.2
         127.0       2.8
         128.0       3.8
         133.0       3.2
         134.0       4.3
         135.0       2.4
         136.0       2.6
         160.0       1.0
         161.0     100.0
         162.0       7.5
         163.0      64.0
         164.0       4.6
         165.0      10.2
    

90 MHz in CDCl3


  • 1H NMR 89.56 MHz
    C6 H5 Cl2 N 0.044 g : 0.5 ml CDCl3
    3,5-dichloroaniline
    ChemicalStructure
        Assign.     Shift(ppm)
    A 6.711 B 6.519 C 3.8

         Hz     ppm     Int.
    

        603.06   6.734    190
        601.25   6.714    367
        599.56   6.695    297
        584.75   6.530   1000
        583.00   6.510    817
        581.44   6.493     42
        338.44   3.779     43
    

in CDCl3



CCl4 solution



KBr disc



nujol mull





OXIDATION WITH PERBENZOIC ACID