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网站主页CAS数据库列表 618-40-6更多图谱1-甲基-1-苯肼(618-40-6)红外图谱(IR2)

1-甲基-1-苯肼

产品名称 1-甲基-1-苯肼

CAS号618-40-6

分子式C7H10N2

分子量122.17

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  • Mass

    MS-KW-0242          
    1-methyl-1-phenylhydrazine
    C7H10N2             (Mass of molecular ion:    122)
    

       Source Temperature: 240 °C
       Sample Temperature: 150 °C
       Reservoir, 75 eV
    

          15.0       1.8
          16.0       1.0
          17.0       1.1
          18.0       1.9
          27.0       3.3
          28.0       5.1
          29.0       9.6
          30.0       2.2
          37.0       1.4
          38.0       3.2
          39.0       9.8
          40.0       1.0
          41.0       1.0
          42.0       1.1
          43.0       4.9
          45.0       1.8
          50.0       8.2
          51.0      23.9
          52.0       7.3
          52.5       1.1
          53.0       4.1
          53.5       1.7
          61.0       3.9
          62.0       1.4
          63.0       5.2
          64.0       3.7
          65.0       8.3
          66.0       2.8
          74.0       2.7
          75.0       2.0
          76.0       2.2
          77.0      90.2
          78.0      17.3
          79.0      21.9
          80.0       2.5
          90.0       1.0
          91.0       4.3
          92.0       6.9
          93.0       7.6
          94.0       2.0
         104.0      11.6
         105.0      10.7
         106.0      25.0
         107.0      68.5
         108.0       5.4
         121.0       8.6
         122.0     100.0
         123.0       8.7
         133.0       3.4
         134.0       3.9
    

400 MHz in CDCl3

90 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C7H10N2 0.05 ml : 0.5 ml CDCl3
    1-methyl-1-phenylhydrazine
    ChemicalStructure
        Assign.     Shift(ppm)
    A 7.208 B 6.924 C 6.765 D 3.56 E 2.983

         Hz     ppm     Int.
    

       2892.09   7.235     40
       2889.90   7.229    213
       2888.92   7.227     99
       2887.70   7.224     87
       2884.89   7.217     53
       2882.57   7.211    264
       2881.72   7.209    180
       2880.99   7.207    274
       2878.79   7.201     55
       2875.86   7.194     94
       2874.52   7.191    102
       2873.66   7.189    249
       2871.46   7.183     44
       2774.42   6.940     61
       2772.34   6.935    264
       2771.25   6.932    310
       2770.39   6.930    180
       2769.05   6.927    105
       2765.51   6.918     93
       2764.53   6.916    152
       2763.43   6.913    260
       2762.46   6.910    235
       2760.01   6.904     42
       2712.41   6.785     68
       2711.31   6.782    116
       2710.33   6.780     70
       2705.08   6.767    112
       2704.11   6.764    195
       2703.01   6.762    111
       2697.76   6.749     57
       2696.78   6.746     99
       2695.68   6.743     60
       1421.03   3.555    153
       1192.27   2.983   1000
    


  • 1H NMR 89.56 MHz
    C7 H10 N2 0.04 ml : 0.5 ml CDCl3
    1-methyl-1-phenylhydrazine
    ChemicalStructure
        Assign.     Shift(ppm)
    A 7.23 B 6.98 C 6.80 D 3.59 E 3.061

         Hz     ppm     Int.
    

        657.69   7.344     31
        656.94   7.336     38
        650.50   7.264     64
        649.25   7.250     65
        648.75   7.244     72
        648.13   7.237     85
        643.81   7.189     65
        642.25   7.172     57
        641.81   7.167     88
        641.13   7.159     91
        628.75   7.021     96
        627.31   7.005    134
        624.94   6.978     32
        621.13   6.936     30
        619.88   6.922     67
        618.50   6.906     58
        615.81   6.876     41
        614.63   6.863     40
        607.50   6.784     59
        600.50   6.706     31
        321.13   3.586     92
        274.13   3.061   1000
    

in CDCl3



KBr disc



liquid film