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网站主页CAS数据库列表 609-67-6更多图谱邻碘苯甲酰氯(609-67-6)质谱(MS)

邻碘苯甲酰氯

产品名称 邻碘苯甲酰氯

CAS号609-67-6

分子式C7H4ClIO

分子量266.46

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  • Mass

    MS-IW-3828          
    o-iodobenzoyl chloride
    C7H4ClIO            (Mass of molecular ion:    266)
    

       Source Temperature: 220 °C
       Sample Temperature: 150 °C
       Reservoir, 75 eV
    

          49.0       1.0
          50.0      10.0
          73.0       1.1
          74.0       5.2
          75.0       6.8
          76.0      20.2
          77.0       1.7
         104.0       2.7
         111.0       2.0
         115.5       3.4
         127.0       2.8
         203.0      24.3
         204.0       1.7
         231.0     100.0
         232.0       7.8
         266.0      13.3
         267.0       1.0
         268.0       4.4
    

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C7 H4 Cl I O 0.040 g : 0.5 ml CDCl3
    o-iodobenzoyl chloride
    ChemicalStructure
        Assign.     Shift(ppm)
    A 8.080 B 8.050 C 7.505 D 7.254

         Hz     ppm     Int.
    

       3234.50   8.094    739
       3234.13   8.093    750
       3232.79   8.090    805
       3226.20   8.073    850
       3224.85   8.070    870
       3221.80   8.062    838
       3220.95   8.060    960
       3216.55   8.049     57
       3214.23   8.043    865
       3213.87   8.042    903
       3213.01   8.040   1000
       3206.79   8.024     31
       3008.06   7.527    569
       3006.84   7.524    579
       3000.61   7.509    793
       3000.12   7.507    723
       2999.39   7.506    816
       2998.90   7.504    653
       2992.68   7.489    632
       2991.46   7.486    641
       2909.06   7.280     52
       2907.47   7.276    659
       2905.88   7.272    631
       2900.02   7.257    753
       2899.54   7.256    742
       2898.44   7.253    715
       2897.95   7.252    698
       2894.41   7.243     45
       2893.68   7.241     59
       2892.09   7.237    554
       2890.50   7.233    577
    

liquid film