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网站主页CAS数据库列表 5932-53-6更多图谱6-羟基托品酮(5932-53-6)核磁图(1HNMR)

6-羟基托品酮

产品名称 6-羟基托品酮

CAS号5932-53-6

分子式C8H13NO2

分子量155.19


  • Mass

    MS-NW-8076          
    6-hydroxy-8-methyl-8-azabicyclo(3.2.1)octan-3-one
    C8H13NO2            (Mass of molecular ion:    155)
    

       Source Temperature: 140 °C
       Sample Temperature: 110 °C
       Direct, 75 eV
    

          15.0       7.4
          18.0       2.2
          26.0       1.1
          27.0       7.5
          28.0      10.8
          29.0       5.2
          30.0       3.8
          31.0       2.0
          39.0       6.0
          40.0       1.5
          41.0      15.9
          42.0      77.0
          43.0       7.4
          44.0       5.9
          53.0       2.5
          54.0       5.5
          55.0      12.7
          56.0       9.0
          57.0      16.4
          58.0       9.7
          67.0       2.3
          68.0       5.0
          69.0       5.5
          70.0       6.5
          71.0       2.0
          72.0       3.2
          80.0       1.7
          81.0       2.7
          82.0      39.9
          83.0      85.3
          84.0       9.6
          86.0       1.3
          94.0       7.2
          95.0       1.5
          96.0      12.7
          97.0      21.7
          98.0      17.3
          99.0       1.2
         110.0      11.9
         111.0     100.0
         112.0      18.3
         113.0       2.0
         126.0       3.7
         138.0       3.3
         155.0      45.3
         156.0       5.8
    

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C8 H13 N O2 0.030 g : 0.5 ml CDCl3
    6-hydroxy-8-methyl-8-azabicyclo(3.2.1)octan-3-one
    ChemicalStructure
        Assign.     Shift(ppm)
    A 4.067 B 3.597 C 3.383 D 3.1 E 2.68 F 2.655 G *1 2.206 J *1 2.095 K 2.055 L 1.994 ASSIGNED BY C-H COSY

         Hz     ppm     Int.
    

       1630.49   4.080     69
       1627.93   4.074     74
       1623.54   4.063     74
       1620.85   4.056     71
       1441.53   3.607     34
       1437.99   3.599     45
       1436.65   3.595     47
       1435.06   3.591     38
       1432.62   3.585     36
       1431.27   3.582     32
       1354.74   3.390     68
       1349.61   3.377     70
       1085.33   2.716     38
       1080.69   2.705     85
       1075.32   2.691     56
       1071.17   2.681     38
       1069.21   2.676     43
       1064.33   2.664    116
       1061.04   2.655   1000
        891.24   2.231     47
        889.40   2.226     82
        887.57   2.221     49
        874.88   2.190     38
        873.17   2.185     70
        871.34   2.181     42
        848.02   2.122     48
        846.07   2.118     79
        844.12   2.113     42
        836.18   2.093     31
        832.28   2.083     45
        830.20   2.078     88
        828.25   2.073     57
        821.90   2.057     73
        814.82   2.039     70
        805.42   2.016     49
        803.34   2.011     31
        798.34   1.998     46
    

in CDCl3



KBr disc



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