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2-氨基-5-氯苯甲腈

产品名称 2-氨基-5-氯苯甲腈

CAS号5922-60-1

分子式C7H5ClN2

分子量152.58


  • Mass

    MS-NW-8846          
    2-amino-5-chlorobenzonitrile
    C7H5ClN2            (Mass of molecular ion:    152)
    

       Source Temperature: 280 °C
       Sample Temperature: 140 °C
       Reservoir, 75 eV
    

          28.0       2.1
          37.0       1.4
          38.0       2.5
          39.0       2.8
          41.0       1.9
          44.5       1.0
          49.0       1.0
          50.0       1.6
          51.0       1.3
          52.0       3.3
          58.5       2.7
          61.0       2.1
          62.0       4.1
          62.5       1.1
          63.0       9.8
          64.0       3.4
          65.0       2.6
          66.0       1.3
          73.0       2.4
          74.0       1.1
          75.0       2.1
          76.0       2.8
          77.0       1.1
          87.0       1.3
          88.0       2.9
          89.0       3.9
          90.0      13.7
          91.0       1.3
          97.0       1.2
          98.0       4.3
          99.0       1.4
         100.0       2.0
         116.0       2.4
         117.0       9.7
         124.0       4.3
         125.0      21.3
         126.0       2.9
         127.0       6.9
         151.0       1.5
         152.0     100.0
         153.0       9.0
         154.0      32.0
         155.0       2.7
    

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C7 H5 Cl N2 0.031 g : 0.5 ml CDCl3
    2-amino-5-chlorobenzonitrile
    ChemicalStructure
        Assign.     Shift(ppm)
    A 7.335 B 7.273 C 6.698 D 4.48

         Hz     ppm     Int.
    

       2932.98   7.339    831
       2930.54   7.333   1000
       2923.46   7.316     23
       2917.11   7.300     23
       2916.75   7.299     23
       2912.48   7.288    552
       2910.03   7.282    452
       2903.69   7.266    588
       2901.25   7.260    506
       2681.27   6.710    947
       2672.36   6.687    890
       1791.14   4.482    301
    

in CDCl3



KBr disc



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