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(S)-(+)-2-氨基-1-丁醇

产品名称 (S)-(+)-2-氨基-1-丁醇

CAS号5856-62-2

分子式C4H11NO

分子量89.14

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  • Mass

    MS-NW-6037          
    (+)-2-amino-1-butanol
    C4H11NO             (Mass of molecular ion:     89)
    

       Source Temperature: 250 °C
       Sample Temperature: 190 °C
       Reservoir, 75 eV
    

          15.0       3.7
          18.0       5.4
          26.0       1.2
          27.0       4.6
          28.0      10.2
          29.0       3.2
          30.0      16.1
          31.0       3.7
          39.0       3.0
          41.0      26.7
          42.0      15.6
          43.0       8.3
          44.0       2.2
          54.0       1.3
          56.0       5.3
          57.0       1.8
          58.0     100.0
          59.0       4.6
          60.0      19.0
          70.0       1.8
    

400 MHz in CDCl3

90 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C4 H11 N O 0.05 ml : 0.5 ml CDCl3
    (+)-2-amino-1-butanol
    ChemicalStructure
        Assign.     Shift(ppm)
    A *1 3.568 B *1 3.28 C 3.25 D 2.734 E *2 1.440 F *2 1.289 G 0.938

         Hz     ppm     Int.
    

       1430.79   3.581     72
       1419.92   3.553     82
       1104.37   2.764     30
       1096.68   2.745     75
       1091.19   2.731     82
       1087.40   2.721     75
       1079.96   2.703     32
        590.58   1.478     58
        584.72   1.464     85
        583.13   1.460     72
        577.15   1.445    132
        571.17   1.430     96
        569.46   1.425    109
        563.60   1.411     86
        562.01   1.407     46
        556.15   1.392     32
        528.44   1.323    106
        521.00   1.304    166
        514.53   1.288    105
        513.55   1.285    132
        507.20   1.270    117
        499.88   1.251     80
        381.96   0.956    589
        374.51   0.938   1000
        366.94   0.919    496
    


  • 1H NMR 89.56 MHz
    C4 H11 N O 0.05 ml : 0.5 ml CDCl3
    (+)-2-amino-1-butanol
    ChemicalStructure
        Assign.     Shift(ppm)
    A *1 3.55 B *1 3.274 C 2.83 D 2.74 E 1.34 F 0.945 J(A,B)=-10.6HZ, J(A,D)=3.9HZ, J(B,D)=7.5HZ

         Hz     ppm     Int.
    

        327.34   3.655     81
        323.34   3.611     97
        316.60   3.536    178
        312.70   3.492    189
        301.46   3.367    330
        294.04   3.284    402
        290.92   3.249    176
        283.40   3.165    232
        277.93   3.104     40
        275.49   3.077     32
        274.32   3.063     34
        273.93   3.059     35
        273.05   3.049     35
        272.07   3.038     37
        270.80   3.024     40
        270.21   3.018     42
        270.02   3.015     42
        269.53   3.010     42
        267.97   2.993     46
        253.81   2.834    802
        245.41   2.741    274
        243.75   2.722    270
        239.45   2.674    206
        236.52   2.641    144
        232.23   2.594     97
        227.83   2.544     39
        226.95   2.535     38
        225.78   2.521     33
        225.10   2.514     31
        224.71   2.510     31
        146.29   1.634     34
        141.11   1.576     68
        138.48   1.547     53
        134.47   1.502    114
        132.81   1.483    177
        131.15   1.465     76
        126.95   1.418    302
        125.00   1.396    231
        121.39   1.356    193
        119.53   1.335    404
        112.79   1.260    284
        106.74   1.192    155
        103.13   1.152     44
        100.68   1.125     81
         99.22   1.108     80
         97.95   1.094     42
         97.46   1.089     41
         94.34   1.054    113
         90.82   1.015    818
         83.40   0.932   1000
         77.64   0.867    286
         76.37   0.853    365
         74.51   0.832    232
         71.48   0.799     57
         69.14   0.772     39
         67.77   0.757     35
         67.09   0.750     34
    

in CDCl3



liquid film



4880 A,200 M,liquid