图谱信息 供应商 相关产品
网站主页CAS数据库列表 583-68-6更多图谱2-溴-4-甲基苯胺(583-68-6)核磁图(13CNMR)

2-溴-4-甲基苯胺

产品名称 2-溴-4-甲基苯胺

CAS号583-68-6

分子式C7H8BrN

分子量186.05

展开


  • Mass

    MS-NW-1580          
    2-bromo-p-toluidine
    C7H8BrN             (Mass of molecular ion:    185)
    

       Source Temperature: 240 °C
       Sample Temperature: 180 °C
       Reservoir, 75 eV
    

          18.0       1.2
          26.0       1.5
          27.0       4.9
          28.0       5.6
          30.0       2.2
          37.0       1.8
          38.0       3.5
          39.0       7.1
          39.5       1.4
          40.0       1.7
          41.0       2.0
          42.0       1.3
          49.0       1.2
          50.0       7.2
          51.0      16.2
          51.5       2.6
          52.0      15.5
          52.5      11.4
          53.0      15.4
          54.0       2.6
          61.0       1.4
          62.0       2.8
          63.0       4.8
          64.0       1.8
          65.0       3.0
          66.0       1.9
          74.0       1.7
          75.0       2.0
          76.0       3.2
          77.0      24.6
          78.0      15.9
          79.0      15.5
          80.0       2.6
          89.0       1.8
          91.0       1.2
          92.5       2.9
          93.5       2.6
         104.0      17.5
         105.0      13.3
         106.0      92.9
         107.0       9.1
         184.0      44.0
         185.0     100.0
         186.0      49.3
         187.0      96.5
         188.0       7.6
    

90 MHz in CDCl3


  • 1H NMR 89.56 MHz
    C7 H8 Br N 0.04 ml : 0.5 ml CDCl3
    2-bromo-p-toluidine
    ChemicalStructure
        Assign.     Shift(ppm)
    A 7.213 B 6.877 C 6.647 D 3.87 E 2.202

         Hz     ppm     Int.
    

        647.25   7.228    127
        646.56   7.220    179
        645.69   7.210    158
        645.31   7.206    149
        644.94   7.202    149
        622.56   6.952     71
        621.88   6.944     70
        621.25   6.937     46
        620.63   6.930     62
        620.00   6.923     57
        615.06   6.868     46
        614.50   6.862    127
        613.81   6.854    133
        613.19   6.847     88
        612.56   6.840    124
        611.88   6.833    120
        611.31   6.826     47
        598.00   6.678    315
        589.94   6.588    157
        346.69   3.872    509
        197.19   2.202   1000
    

in CDCl3



CCl4 solution



liquid film