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网站主页CAS数据库列表 555-57-7更多图谱优降宁(555-57-7)核磁图(1HNMR)

优降宁

产品名称 优降宁

CAS号555-57-7

分子式C11H13N

分子量159.23

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  • Mass

    MS-NW-5455          
    N-methyl-N-(2-propynyl)benzylamine
    C11H13N             (Mass of molecular ion:    159)
    

       Source Temperature: 260 °C
       Sample Temperature: 190 °C
       Reservoir, 75 eV
    

          15.0       4.6
          18.0       1.3
          27.0       2.0
          28.0       2.7
          37.0       1.1
          38.0       3.1
          39.0      21.1
          40.0       2.7
          41.0       8.5
          42.0      43.9
          43.0       2.1
          44.0       3.8
          50.0       3.2
          51.0       7.7
          52.0       2.1
          55.0       1.0
          62.0       1.6
          63.0       5.6
          64.0       1.8
          65.0      21.0
          66.0       3.8
          68.0      66.9
          69.0       3.4
          76.0       1.0
          77.0       5.7
          78.0       2.4
          78.5       1.4
          79.0       1.7
          80.0       3.4
          81.0       1.8
          82.0     100.0
          83.0       6.3
          89.0       4.8
          90.0       2.2
          91.0      96.3
          92.0      30.5
          93.0       2.3
         104.0       2.2
         115.0       3.8
         116.0       1.8
         117.0       1.9
         118.0      12.0
         119.0       2.6
         120.0       2.9
         128.0       1.2
         129.0       1.1
         132.0       5.8
         134.0       3.8
         143.0       1.2
         144.0       1.5
         157.0       1.5
         158.0      32.5
         159.0      41.9
         160.0       6.3
    

90 MHz in CDCl3


  • 1H NMR 89.56 MHz
    C11 H13 N 0.04 ml : 0.5 ml CDCl3
    N-methyl-N-(2-propynyl)benzylamine
    ChemicalStructure
        Assign.     Shift(ppm)
    A 7.59 to 7.03 B 3.563 C 3.295 D 2.332 E 2.254 J(C,E)=2.4HZ.

         Hz     ppm     Int.
    

        660.56   7.376     60
        658.38   7.352     36
        656.44   7.330    154
        653.94   7.302    821
        651.25   7.272    194
        649.31   7.251     51
        647.63   7.232     74
        646.19   7.216     29
        645.81   7.211     29
        319.19   3.564    624
        296.44   3.310    317
        294.06   3.284    340
        208.94   2.333   1000
        204.25   2.281    191
        201.88   2.255    390
        199.44   2.227    195
    

in CDCl3



liquid film



4880 A,200 M,liquid