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网站主页CAS数据库列表 5284-29-7更多图谱2-十二烷基酚(5284-29-7)核磁图(13CNMR)

2-十二烷基酚

产品名称 2-十二烷基酚

CAS号5284-29-7

分子式C18H30O

分子量262.43


  • Mass

    MS-IW-0527          
    o-dodecylphenol
    C18H30O             (Mass of molecular ion:    262)
    

       Source Temperature: 160 °C
       Sample Temperature: 130 °C
       Direct, 75 eV
    

          29.0       1.6
          41.0       3.2
          43.0       4.1
          55.0       2.1
          57.0       2.8
          71.0       1.0
          77.0       3.5
          79.0       2.4
          91.0       1.2
          94.0       5.9
          95.0       1.1
          96.0       1.5
         107.0     100.0
         108.0      22.3
         109.0       2.9
         120.0       3.6
         121.0       3.3
         122.0       2.1
         133.0       2.1
         136.0       1.0
         149.0       1.1
         262.0      51.0
         263.0      10.1
         264.0       1.0
    

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C18 H30 O 0.035 g : 0.5 ml CDCl3
    o-dodecylphenol
    ChemicalStructure
        Assign.     Shift(ppm)
    A 7.111 B 7.067 C 6.864 D 6.748 E 4.75 F 2.589 G 1.601 J 1.31 K 1.26 L 0.878

         Hz     ppm     Int.
    

       2846.68   7.123     58
       2845.21   7.120     68
       2839.23   7.105     67
       2837.77   7.101     81
       2833.25   7.090     44
       2831.54   7.086     38
       2825.68   7.071     78
       2824.10   7.067     67
       2817.99   7.052     58
       2816.28   7.047     49
       2750.61   6.883     60
       2749.39   6.880     64
       2743.16   6.864    101
       2742.07   6.862    107
       2735.84   6.846     45
       2734.62   6.843     47
       2701.29   6.760     98
       2700.20   6.757     96
       2693.24   6.739     87
       2692.26   6.737     85
       1897.22   4.748    350
       1042.97   2.610    102
       1035.28   2.591    121
       1027.34   2.571    112
        648.68   1.624     41
        641.24   1.605     69
        633.67   1.586     55
        549.56   1.376     31
        547.85   1.371     32
        547.24   1.370     32
        546.39   1.368     31
        541.63   1.356     51
        537.60   1.346     57
        534.42   1.338     73
        529.17   1.325     92
        526.61   1.318     85
        523.68   1.311     76
        523.19   1.310     76
        519.17   1.300     96
        511.11   1.279    138
        510.74   1.278    137
        501.71   1.256   1000
        358.28   0.897    125
        351.56   0.880    409
        344.48   0.862    154
    

in CDCl3



KBr disc



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