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网站主页CAS数据库列表 5159-41-1更多图谱2-碘苄醇(5159-41-1)核磁图(1HNMR)

2-碘苄醇

产品名称 2-碘苄醇

CAS号5159-41-1

分子式C7H7IO

分子量234.03

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  • Mass

    MS-NW-6613          
    o-iodobenzyl alcohol
    C7H7IO              (Mass of molecular ion:    234)
    

       Source Temperature: 260 °C
       Sample Temperature: 190 °C
       Reservoir, 75 eV
    

          18.0       1.5
          27.0       5.0
          28.0       1.5
          29.0       4.6
          31.0       3.3
          37.0       2.1
          38.0       3.2
          39.0       9.3
          40.0       1.0
          49.0       1.7
          50.0      17.0
          51.0      23.5
          52.0       7.0
          53.0       5.1
          61.0       1.6
          62.0       3.8
          63.0       6.7
          64.0       1.7
          73.0       1.3
          74.0       6.1
          75.0       4.5
          76.0      11.5
          77.0      59.1
          78.0      42.5
          79.0      72.2
          80.0       4.9
          89.0       9.0
          90.0       8.2
          91.0       1.5
         104.0       1.6
         105.0      34.8
         106.0       5.6
         107.0      37.2
         108.0       3.4
         127.0       5.9
         128.0       2.8
         203.0       3.3
         205.0       2.1
         217.0       3.3
         218.0       1.1
         231.0       1.9
         232.0       1.2
         233.0       5.8
         234.0     100.0
         235.0       8.0
    

90 MHz in CDCl3


  • 1H NMR 89.56 MHz
    C7 H7 I O 0.039 g : 0.5 ml CDCl3
    o-iodobenzyl alcohol
    ChemicalStructure
        Assign.     Shift(ppm)
    A 7.804 B 7.44 C 7.35 D 6.98 E 4.649 F 2.15

         Hz     ppm     Int.
    

        703.50   7.856    158
        702.44   7.844    140
        695.88   7.770    178
        694.81   7.759    188
        664.50   7.420    343
        663.38   7.408    319
        662.88   7.402    252
        662.38   7.396    240
        657.94   7.347    220
        656.75   7.334    205
        649.19   7.249    161
        633.06   7.069    112
        630.50   7.040     96
        626.44   6.995     85
        625.25   6.982     97
        623.88   6.967     86
        416.44   4.650   1000
        192.81   2.153    325
    

in CDCl3



KBr disc



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