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网站主页CAS数据库列表 50816-20-1更多图谱1-溴-8-(四氢吡喃氧基)辛烷, TECH(50816-20-1)核磁图(1HNMR)

1-溴-8-(四氢吡喃氧基)辛烷, TECH

产品名称 1-溴-8-(四氢吡喃氧基)辛烷, TECH

CAS号50816-20-1

分子式C13H25BrO2

分子量293.24

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  • Mass

    MS-NW-6120          
    2-(8-bromooctyloxy)tetrahydropyran
    C13H25BrO2          (Mass of molecular ion:    292)
    

       Source Temperature: 250 °C
       Sample Temperature: 190 °C
       Reservoir, 75 eV
    

          27.0       7.9
          28.0       4.2
          29.0      10.8
          31.0       3.9
          39.0       5.3
          40.0       1.2
          41.0      27.2
          42.0       4.6
          43.0      10.7
          44.0       1.6
          53.0       2.1
          54.0       3.6
          55.0      27.6
          56.0      29.5
          57.0      16.4
          67.0       7.0
          68.0       4.0
          69.0      28.3
          70.0       2.5
          71.0       2.8
          81.0       1.9
          82.0       2.4
          83.0       6.0
          84.0       9.1
          85.0     100.0
          86.0       6.4
         101.0       6.5
         102.0       1.2
         111.0       6.2
         115.0       1.8
         135.0       2.5
         137.0       2.2
         148.0       2.0
         149.0       1.2
         150.0       2.1
         151.0       1.2
         162.0       1.7
         164.0       1.6
         191.0       1.0
         193.0       1.0
         291.0       1.0
         293.0       1.0
    

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C13 H25 Br O2 0.04 ml : 0.5 ml CDCl3
    2-(8-bromooctyloxy)tetrahydropyran
    ChemicalStructure
        Assign.     Shift(ppm)
    A 4.574 B 3.870 C 3.730 D 3.505 E 3.405 F 3.383 G 1.853 J 1.71 K 1.59 to 1.55 L 1.43 M 1.34

         Hz     ppm     Int.
    

       1831.79   4.584    152
       1829.10   4.577    230
       1827.39   4.573    169
       1824.58   4.566    166
       1546.51   3.870    140
       1496.09   3.744    234
       1493.41   3.737    138
       1489.26   3.727    132
       1486.57   3.720    258
       1479.61   3.703    129
       1367.80   3.423    501
       1362.06   3.409    288
       1360.84   3.406   1000
       1356.20   3.394    316
       1354.00   3.388    559
       1349.61   3.377    165
       1346.68   3.370    240
        747.68   1.871    301
        740.60   1.854    361
        734.62   1.839    212
        732.91   1.834    321
        726.07   1.817    204
        683.11   1.710    136
        644.78   1.614    183
        644.53   1.613    183
        643.19   1.610    190
        636.72   1.594    323
        635.86   1.592    309
        631.23   1.580    315
        627.44   1.570    205
        623.78   1.561    250
        619.51   1.551    244
        617.68   1.546    276
        616.70   1.544    287
        614.14   1.537    292
        608.52   1.523    179
        607.54   1.521    169
        605.96   1.517    141
        571.17   1.430    189
        535.16   1.340    700
    

in CDCl3



liquid film