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网站主页CAS数据库列表 504-24-5更多图谱4-氨基吡啶(504-24-5)核磁图(13CNMR)

4-氨基吡啶

产品名称 4-氨基吡啶

CAS号504-24-5

分子式C5H6N2

分子量94.11

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  • Mass

    MS-NW-1397          
    4-pyridylamine
    C5H6N2              (Mass of molecular ion:     94)
    

       Source Temperature: 260 °C
       Sample Temperature: 180 °C
       Reservoir, 75 eV
    

          18.0       1.2
          26.0       3.2
          27.0       1.3
          28.0       8.9
          30.0       1.1
          37.0       2.2
          38.0       4.5
          39.0      13.1
          40.0      10.0
          41.0      26.3
          42.0       5.6
          43.0       1.9
          46.5       1.0
          47.0       1.3
          50.0       2.8
          51.0       4.0
          52.0       6.1
          53.0       1.7
          54.0       5.3
          65.0       2.1
          66.0       8.8
          67.0      37.6
          68.0       4.9
          93.0       8.1
          94.0     100.0
          95.0       6.4
    

400 MHz in DMSO-d6


  • 1H NMR 399.65 MHz
    C5 H6 N2 0.040 g : 0.5 ml DMSO-d6
    4-pyridylamine
    ChemicalStructure
        Assign.     Shift(ppm)
    A 7.987 B 6.476 C 6.03

         Hz     ppm     Int.
    

       3194.95   7.995    545
       3188.96   7.980    532
       2591.43   6.485   1000
       2589.84   6.481    723
       2586.67   6.473    698
       2585.08   6.469    934
       2408.08   6.026    506
    

in CDCl3

in DMSO-d6





KBr disc



nujol mull