图谱信息 供应商 相关产品
网站主页CAS数据库列表 480-22-8更多图谱1,8,9-三羟基蒽(480-22-8)质谱(MS)

1,8,9-三羟基蒽

产品名称 1,8,9-三羟基蒽

CAS号480-22-8

分子式C14H10O3

分子量226.23

展开


  • Mass

    MS-NW-7088          
    1,8,9-anthracenetriol
    C14H10O3            (Mass of molecular ion:    226)
    

       Source Temperature: 200 °C
       Sample Temperature: 120 °C
       Direct, 75 eV
    

          18.0       1.6
          39.0       2.3
          50.0       1.4
          51.0       2.6
          57.5       1.0
          62.0       1.7
          63.0       4.5
          69.5       1.0
          70.0       1.1
          74.0       1.5
          75.0       3.5
          75.5       3.1
          76.0       9.3
          76.5       1.3
          77.0       1.8
          84.0       2.7
          87.0       1.4
          89.0       1.4
          90.0       1.9
          98.5       2.0
          99.0       2.4
         104.0       2.8
         113.0       3.1
         115.0       4.4
         126.0       1.0
         139.0       3.7
         140.0       1.1
         141.0       4.1
         150.0       3.2
         151.0       7.3
         152.0      10.4
         153.0       2.4
         168.0       1.8
         169.0       4.0
         170.0       1.2
         180.0       6.2
         181.0       5.6
         182.0       1.0
         197.0      15.2
         198.0      15.5
         199.0       2.4
         208.0       1.0
         209.0       1.3
         210.0       2.5
         225.0       5.2
         226.0     100.0
         227.0      15.5
         228.0       1.8
         240.0       1.0
    

400 MHz in CDCl3

90 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C14 H10 O3 0.046 g : 0.5 ml CDCl3
    1,8,9-anthracenetriol
    ChemicalStructure
        Assign.     Shift(ppm)
    A 12.21 B 7.423 C 6.83 D 4.241

         Hz     ppm     Int.
    

       4881.57  12.215     43
       4879.19  12.209   1000
       2974.81   7.444    232
       2966.75   7.424    377
       2963.27   7.415     22
       2959.05   7.405    257
       2742.74   6.863     26
       2741.64   6.861     24
       2740.90   6.859     21
       2732.29   6.837    569
       2725.15   6.819    386
       2724.24   6.817    667
       2723.50   6.815    387
       1694.84   4.241    424
    


  • 1H NMR 89.56 MHz
    C14 H10 O3 0.042 g : 0.5 ml CDCl3
    1,8,9-anthracenetriol
    ChemicalStructure
        Assign.     Shift(ppm)
    A 12.22 B 7.437 C 6.86 D 4.28

         Hz     ppm     Int.
    

       1094.35  12.220   1000
        675.05   7.538    182
        667.79   7.457    256
        666.50   7.442    259
        659.24   7.361    320
        617.63   6.897    661
        616.94   6.889    575
        613.53   6.851     57
        609.68   6.808    526
        609.00   6.800    450
        383.24   4.280    906
        379.31   4.236     52
        378.54   4.227     41
        378.03   4.221     38
    

in CDCl3



KBr disc



nujol mull