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MassMS-NW-9900 5'-fluoro-2'-hydroxyacetophenone C8H7FO2 (Mass of molecular ion: 154)
Source Temperature: 260 °C Sample Temperature: 160 °C Reservoir, 75 eV
15.0 1.1 28.0 1.1 31.0 1.3 39.0 1.5 43.0 17.4 50.0 1.3 51.0 1.8 53.0 1.4 56.0 1.0 57.0 9.1 62.0 1.2 63.0 3.8 69.5 1.6 77.0 1.9 81.0 2.6 82.0 2.9 83.0 20.0 84.0 2.1 95.0 1.0 97.0 1.0 107.0 1.5 108.0 2.0 110.0 1.4 111.0 25.6 112.0 3.8 136.0 1.6 139.0 100.0 140.0 7.7 154.0 62.4 155.0 5.7
400 MHz in CDCl3
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1H NMR 399.65 MHz C8 H7 F O2 0.037 g : 0.5 ml CDCl3 5'-fluoro-2'-hydroxyacetophenone 
Assign. Shift(ppm)
A 12.0 B 7.393 C 7.215 D 6.948 E 2.614
Hz ppm Int.4787.24 11.979 316 2960.70 7.409 71 2957.77 7.401 76 2951.91 7.387 72 2948.98 7.379 77 2894.21 7.242 37 2893.85 7.241 39 2891.10 7.235 37 2890.73 7.234 37 2886.34 7.223 46 2885.97 7.222 47 2885.06 7.219 50 2884.69 7.219 50 2883.22 7.215 42 2882.86 7.214 42 2881.94 7.212 48 2881.58 7.211 47 2877.18 7.200 50 2876.81 7.199 51 2874.07 7.192 44 2873.70 7.191 44 2782.48 6.963 85 2782.12 6.962 83 2777.90 6.951 84 2777.54 6.950 79 2773.32 6.940 73 2772.96 6.939 71 2768.74 6.928 69 1047.53 2.622 31 1044.78 2.615 1000
in CDCl3
KBr disc
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