图谱信息 供应商 相关产品
网站主页CAS数据库列表 3855-32-1更多图谱N-[3-(二甲氨基)丙基]-N,N’,N’-三甲基-1,3丙二胺(3855-32-1)核磁图(1HNMR)

N-[3-(二甲氨基)丙基]-N,N’,N’-三甲基-1,3丙二胺

产品名称 N-[3-(二甲氨基)丙基]-N,N’,N’-三甲基-1,3丙二胺

CAS号3855-32-1

分子式C11H27N3

分子量201.35

展开


  • Mass

    MS-IW-9002          
    N-(3-(dimethylamino)propyl)-N,N',N'-trimethyltrimethylenediamine
    C11H27N3            (Mass of molecular ion:    201)
    

       Source Temperature: 200 °C
       Sample Temperature: 150 °C
       Reservoir, 75 eV
    

          15.0       1.5
          27.0       1.0
          28.0       2.6
          29.0       1.3
          30.0       3.8
          41.0       3.2
          42.0      13.9
          43.0       5.7
          44.0       9.7
          45.0       1.8
          56.0       3.5
          57.0       4.9
          58.0     100.0
          59.0       4.5
          70.0      18.1
          71.0       7.2
          72.0      10.7
          82.0       2.3
          83.0       1.1
          84.0      15.8
          85.0      63.9
          86.0       8.0
          96.0       3.2
          98.0       6.1
         111.0       1.5
         113.0       1.2
         117.0       7.9
         127.0       5.0
         156.0       1.0
         201.0       7.6
         202.0       1.1
    

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C11 H27 N3 0.05 ml : 0.5 ml CDCl3
    N-(3-(dimethylamino)propyl)-N,N',N'-trimethyltrimethylenediamine
    ChemicalStructure
        Assign.     Shift(ppm)
    A 2.357 B 2.274 C 2.219 D 1.640

         Hz     ppm     Int.
    

        952.27   2.383     33
        949.58   2.377    126
        942.02   2.358    136
        939.82   2.352     65
        934.45   2.339    134
        916.14   2.293    134
        908.81   2.275    156
        901.12   2.255    148
        887.08   2.220   1000
        670.17   1.677     40
        664.18   1.662     48
        662.60   1.658     82
        657.47   1.646     52
        655.15   1.640    131
        653.20   1.635     48
        649.17   1.625     46
        647.46   1.621     67
        646.36   1.618     47
        640.14   1.602     33
    

in CDCl3



liquid film