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网站主页CAS数据库列表 372-75-8更多图谱L-瓜氨酸(372-75-8)质谱(MS)

L-瓜氨酸

产品名称 L-瓜氨酸

CAS号372-75-8

分子式C6H13N3O3

分子量175.19

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  • Mass

    MS-NW-0373          
    L-citrulline
    C6H13N3O3           (Mass of molecular ion:    175)
    

       Source Temperature: 180 °C
       Sample Temperature: 270 °C
       Direct, 75 eV
    

          15.0       2.4
          16.0      10.6
          17.0      15.0
          18.0      23.8
          26.0       2.0
          27.0       6.9
          28.0      27.0
          29.0       7.9
          30.0      44.8
          31.0       2.0
          38.0       1.1
          39.0       7.2
          40.0       2.3
          41.0      14.3
          42.0      14.3
          43.0      53.8
          44.0      34.8
          45.0       2.3
          52.0       1.4
          53.0       1.8
          54.0       4.9
          55.0       3.9
          56.0      62.4
          57.0      13.7
          58.0      29.1
          59.0       1.5
          60.0       1.2
          67.0       1.2
          68.0       8.6
          69.0     100.0
          70.0      28.3
          71.0       1.8
          75.0       1.7
          82.0       2.5
          83.0       1.9
          85.0       6.8
          86.0       5.8
          87.0       1.5
          97.0       7.1
          98.0       1.7
          99.0       1.1
         100.0       1.1
         101.0       2.1
         110.0       1.0
         111.0       4.9
         112.0       2.6
         113.0       3.2
         114.0       9.6
         115.0       1.3
         138.0       1.9
         139.0       4.4
         140.0       4.0
         164.0       1.6
         165.0       1.2
         175.0       1.1
    

90 MHz in D2O


  • 1H NMR 89.56 MHz
    C6 H13 N3 O3 0.039 g : 0.5 ml D2O
    L-citrulline
    ChemicalStructure
        Assign.     Shift(ppm)
    B 3.757 C 3.145 D *1 1.85 E *1 1.59 THE SOLVENT SIGNAL REMOVED.

         Hz     ppm     Int.
    

        342.38   3.823    287
        336.63   3.759    669
        330.75   3.694    408
        288.38   3.220    487
        281.75   3.146   1000
        278.31   3.108    275
        275.50   3.077    495
        175.06   1.955    291
        171.75   1.918    265
        169.00   1.888    405
        165.19   1.845    500
        162.94   1.820    456
        159.44   1.781    450
        153.88   1.719    314
        153.75   1.717    314
        148.00   1.653    497
        144.50   1.614    303
        143.38   1.601    356
        142.56   1.592    332
        141.50   1.580    375
        136.88   1.529    320
    

in D2O



KBr disc



nujol mull



4880 A,200 M,powder