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网站主页CAS数据库列表 36822-11-4更多图谱6-苯基-2-硫尿嘧啶(36822-11-4)红外图谱(IR1)

6-苯基-2-硫尿嘧啶

产品名称 6-苯基-2-硫尿嘧啶

CAS号36822-11-4

分子式C10H8N2OS

分子量204.25

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  • Mass

    MS-NW-7196          
    6-phenyl-2-thiouracil
    C10H8N2OS           (Mass of molecular ion:    204)
    

       Source Temperature: 150 °C
       Sample Temperature: 170 °C
       Direct, 75 eV
    

          17.0       1.4
          18.0       6.2
          27.0       1.7
          28.0       2.1
          32.0       1.0
          37.0       1.3
          38.0       2.2
          39.0       6.8
          40.0       3.3
          41.0       1.0
          42.0       2.8
          43.0       1.4
          45.0       1.4
          50.0       8.5
          51.0      15.4
          52.0       4.2
          58.5       1.1
          59.0       2.9
          60.0       2.3
          61.0       1.3
          62.0       3.2
          63.0       7.9
          64.0       1.8
          65.0       1.7
          68.0      11.3
          69.0       5.5
          73.0       1.3
          74.0       4.2
          75.0       4.9
          76.0       7.1
          77.0      23.5
          78.0       4.6
          87.0       1.0
          88.0       5.7
          89.0      12.5
          90.0       6.2
          91.0       1.8
         101.0       1.4
         102.0       6.9
         103.0      11.4
         104.0      57.2
         105.0       7.2
         116.0      10.7
         117.0      13.4
         118.0       2.0
         121.0       2.0
         128.0       1.2
         129.0       3.2
         134.0      15.7
         135.0       1.8
         136.0       1.1
         144.0       2.1
         145.0      14.7
         146.0      16.2
         147.0       1.8
         148.0       1.4
         149.0       2.8
         171.0       4.1
         175.0       1.6
         176.0      26.6
         177.0       3.5
         178.0       1.6
         203.0      10.5
         204.0     100.0
         205.0      13.2
         206.0       5.4
    

400 MHz in DMSO-d6

90 MHz in DMSO-d6


  • 1H NMR 399.65 MHz
    C10 H8 N2 O S 0.040 g : 0.5 ml DMSO-d6
    6-phenyl-2-thiouracil
    ChemicalStructure
        Assign.     Shift(ppm)
    A *1 12.56 B *1 12.49 C 7.711 D 7.554 E 7.504 F 6.096 90MHZ : HSP-04-952

         Hz     ppm     Int.
    

       5019.31  12.560    299
       4993.48  12.495    125
       3086.36   7.723    775
       3079.40   7.706    945
       3077.93   7.702    744
       3069.69   7.681     34
       3029.02   7.580    129
       3027.93   7.577    101
       3024.63   7.569    110
       3021.70   7.561    474
       3019.50   7.556    187
       3015.84   7.547    320
       3014.55   7.543    462
       3013.27   7.540    290
       3010.52   7.533     99
       3005.76   7.521    775
       2998.07   7.502    904
       2992.76   7.489    207
       2991.11   7.485    344
       2989.83   7.482    240
       2983.60   7.466     32
       2436.48   6.097   1000
    


  • 1H NMR 89.56 MHz
    C10 H8 N2 O S 0.036 g : 0.5 ml DMSO-d6
    6-phenyl-2-thiouracil
    ChemicalStructure
        Assign.     Shift(ppm)
    A 12.48 B 7.70 C 7.59 to 7.380 D 6.084

         Hz     ppm     Int.
    

       1117.93  12.483    276
        696.33   7.776    228
        694.27   7.753    306
        690.52   7.711    351
        689.66   7.701    379
        686.50   7.666    594
        684.36   7.642    242
        682.40   7.620    134
        681.29   7.608    152
        679.83   7.591    241
        678.55   7.577    347
        675.73   7.546   1000
        674.02   7.526    868
        670.61   7.488    445
        668.55   7.465    421
        666.08   7.438    144
        665.73   7.434    147
        664.28   7.418    147
        662.66   7.400     81
        662.23   7.395     79
        661.63   7.388     81
        661.29   7.384     74
        660.18   7.372     71
        659.75   7.367     74
        545.00   6.086    615
    

in DMSO-d6



KBr disc



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