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网站主页CAS数据库列表 33786-89-9更多图谱5-氯-m-苯二胺(33786-89-9)质谱(MS)

5-氯-m-苯二胺

产品名称 5-氯-m-苯二胺

CAS号33786-89-9

分子式C6H7ClN2

分子量142.59

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  • Mass

    MS-NW-4691          
    5-chloro-m-phenylenediamine
    C6H7ClN2            (Mass of molecular ion:    142)
    

       Source Temperature: 260 °C
       Sample Temperature: 170 °C
       Reservoir, 75 eV
    

          18.0       1.8
          27.0       1.1
          28.0       3.1
          37.0       1.6
          38.0       3.3
          39.0       4.3
          40.0       2.6
          41.0       3.3
          42.0       3.7
          43.0       1.2
          50.0       2.6
          51.0       6.1
          52.0       7.2
          53.0       8.7
          54.0       2.1
          61.0       1.1
          62.0       2.2
          63.0       4.3
          64.0       1.3
          65.0       2.8
          66.0       4.0
          67.0       3.1
          71.0       4.8
          72.0       1.9
          73.0       1.3
          75.0       1.0
          76.0       1.6
          77.0       1.9
          78.0      12.3
          79.0       5.0
          80.0      34.4
          81.0       2.4
          87.0       1.7
          89.0       1.3
          90.0       3.3
         105.0       3.3
         106.0       3.1
         107.0      12.0
         108.0       1.0
         114.0      14.9
         115.0       6.5
         116.0       5.5
         117.0       2.1
         125.0       3.2
         127.0       1.2
         141.0       4.1
         142.0     100.0
         143.0       8.6
         144.0      31.7
         145.0       2.6
    

90 MHz in CDCl3


  • 1H NMR 89.56 MHz
    C6 H7 Cl N2 0.042 g : 0.5 ml CDCl3
    5-chloro-m-phenylenediamine
    ChemicalStructure
        Assign.     Shift(ppm)
    A 6.083 B 5.839 C 3.56 J(A,B)=2.0HZ.

         Hz     ppm     Int.
    

        546.00   6.097    792
        544.06   6.075   1000
        525.00   5.862    207
        522.94   5.839    329
        521.00   5.818    173
        318.38   3.555    335
    

in CDCl3



KBr disc



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