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网站主页CAS数据库列表 30860-22-1更多图谱3-氯-2-降冰片酮(30860-22-1)核磁图(13CNMR)

3-氯-2-降冰片酮

产品名称 3-氯-2-降冰片酮

CAS号30860-22-1

分子式C7H9ClO

分子量144.6

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  • Mass

    MS-NW-6434          
    endo-3-chloro-2-norbornanone
    C7H9ClO             (Mass of molecular ion:    144)
    

       Source Temperature: 260 °C
       Sample Temperature: 190 °C
       Reservoir, 75 eV
    

          18.0       1.1
          26.0       3.3
          27.0      16.0
          28.0       1.3
          29.0       1.4
          36.0       1.6
          37.0       1.2
          38.0       3.2
          39.0      22.0
          40.0       4.4
          41.0      26.2
          42.0       1.4
          49.0       1.9
          50.0       3.4
          51.0       6.5
          52.0       3.6
          53.0      14.6
          54.0      15.7
          55.0       5.6
          63.0       1.1
          65.0       4.3
          66.0       9.8
          67.0     100.0
          68.0       7.3
          69.0       1.0
          75.0      45.9
          76.0       2.4
          77.0      15.4
          78.0       1.3
          79.0      13.3
          80.0      25.0
          81.0      81.9
          82.0       5.7
          88.0       7.4
          90.0       2.3
         101.0       1.0
         109.0       7.0
         115.0       1.7
         144.0      31.5
         145.0       2.5
         146.0      10.6
    

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C7 H9 Cl O 0.05 ml : 0.5 ml CDCl3
    endo-3-chloro-2-norbornanone
    ChemicalStructure
        Assign.     Shift(ppm)
    A 3.693 B 2.72 C 2.242 D *1 1.961 E *2 1.864 F 1.622 G *2 1.556 J *1 1.509 ASSIGNED BY C-H COSY

         Hz     ppm     Int.
    

       1477.54   3.698    941
       1474.49   3.690   1000
       1092.16   2.733    455
       1089.11   2.726    441
       1087.16   2.721    678
       1085.82   2.717    780
       1084.59   2.714    594
       1082.89   2.710    411
       1081.30   2.706    546
       1080.20   2.703    538
        903.56   2.261    264
        901.86   2.257    388
        900.27   2.253    294
        898.32   2.248    137
        892.70   2.234    292
        891.11   2.230    429
        889.40   2.226    326
        887.57   2.221    146
        800.66   2.004    161
        796.14   1.993    145
        791.87   1.982    355
        786.99   1.970    350
        783.33   1.961    225
        779.54   1.951    231
        776.25   1.943    250
        774.78   1.939    259
        771.61   1.931    222
        760.25   1.903    168
        756.47   1.893    277
        752.08   1.882    174
        748.41   1.873    199
        744.02   1.862    407
        739.87   1.852    279
        735.47   1.841    126
        731.08   1.830    149
        656.62   1.643    242
        655.40   1.640    309
        654.79   1.639    325
        653.56   1.636    476
        652.34   1.633    347
        651.86   1.632    333
        650.51   1.628    284
        645.87   1.617    240
        644.53   1.613    300
        643.92   1.612    310
        642.82   1.609    453
        641.60   1.606    333
        640.99   1.604    320
        639.77   1.601    270
        635.25   1.590    169
        633.06   1.585    184
        629.76   1.576    125
        626.46   1.568    224
        624.15   1.562    260
        623.05   1.559    358
        620.85   1.554    332
        613.65   1.536    766
        611.45   1.530    866
        604.25   1.512    263
        602.05   1.507    294
        600.34   1.503    260
        598.02   1.497    214
        591.67   1.481    142
        589.36   1.475    132
    

in CDCl3



liquid film