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网站主页CAS数据库列表 30727-14-1更多图谱1-乙基-3-羟基-四氢吡咯(30727-14-1)核磁图(1HNMR)

1-乙基-3-羟基-四氢吡咯

产品名称 1-乙基-3-羟基-四氢吡咯

CAS号30727-14-1

分子式C6H13NO

分子量115.17

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  • Mass

    MS-NW-3437          
    1-ethyl-3-pyrrolidinol
    C6H13NO             (Mass of molecular ion:    115)
    

       Source Temperature: 270 °C
       Sample Temperature: 180 °C
       Reservoir, 75 eV
    

          14.0       1.6
          15.0      11.8
          17.0       1.4
          18.0       4.5
          26.0       8.1
          27.0      37.0
          28.0      34.4
          29.0      23.1
          30.0      23.5
          31.0       6.4
          37.0       1.8
          38.0       3.9
          39.0      16.6
          40.0       6.1
          41.0      26.3
          42.0      85.4
          43.0     100.0
          44.0      27.8
          45.0       1.4
          50.0       2.5
          51.0       4.4
          52.0       2.9
          53.0       4.8
          54.0       6.3
          55.0       7.3
          56.0      17.7
          57.0       9.0
          58.0      22.5
          59.0       1.6
          63.0       1.5
          65.0       4.5
          66.0       1.5
          67.0       4.8
          68.0      12.7
          69.0       2.4
          70.0       7.5
          71.0      55.4
          72.0       6.8
          77.0       1.8
          78.0       1.3
          79.0       1.5
          80.0       9.8
          81.0       1.5
          82.0      18.4
          83.0       1.4
          84.0       1.9
          85.0       1.9
          86.0       2.3
          89.0       1.0
          91.0      29.8
          92.0       2.9
          93.0       1.0
          94.0       1.9
          95.0       6.1
          96.0      11.0
          97.0       6.2
          98.0       2.3
         100.0      76.0
         101.0       4.5
         114.0       9.8
         115.0      23.2
         116.0       1.7
         120.0       3.9
         134.0       1.9
         135.0       1.1
         148.0       3.5
         157.0       2.1
    

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C6 H13 N O 0.05 ml : 0.5 ml CDCl3
    1-ethyl-3-pyrrolidinol
    ChemicalStructure
        Assign.     Shift(ppm)
    A 4.9 B 4.332 C *1 2.789 D 2.631 E 2.577 F 2.488 G *1 2.365 J *2 2.174 K *2 1.714 L 1.109 J(D,E)=10.2HZ. J(D,B)=5.9HZ. J(E,B)=3.1HZ.

         Hz     ppm     Int.
    

       1740.97   4.357     53
       1737.92   4.349     98
       1734.99   4.342     98
       1733.28   4.337     80
       1732.18   4.335    109
       1730.22   4.330    110
       1729.13   4.327     79
       1727.42   4.323     94
       1724.49   4.316     90
       1721.31   4.308     46
       1126.22   2.819     67
       1120.61   2.804     79
       1117.43   2.797    105
       1111.69   2.782    110
       1109.01   2.775     83
       1103.27   2.761     74
       1061.28   2.656    113
       1055.42   2.641    112
       1051.03   2.630    230
       1045.29   2.616    229
       1034.79   2.590    182
       1031.62   2.582    180
       1024.54   2.564     90
       1021.48   2.556     85
       1005.86   2.517    122
       1005.00   2.515    122
        998.54   2.499    343
        997.80   2.497    333
        991.21   2.481    350
        990.60   2.479    350
        987.06   2.470     38
        983.40   2.461    138
        957.15   2.395     77
        950.68   2.379     95
        948.73   2.374    121
        942.26   2.358    122
        939.58   2.352     95
        933.23   2.336     86
        886.23   2.218     51
        880.62   2.204     57
        878.30   2.198     74
        872.80   2.184    121
        870.36   2.178     55
        867.07   2.170     69
        864.75   2.164    114
        859.25   2.151     79
        856.81   2.144     52
        851.20   2.130     42
        699.34   1.750     45
        696.53   1.743     47
        692.87   1.734     54
        691.04   1.730     63
        688.60   1.724     57
        685.55   1.716     68
        682.50   1.708     67
        679.32   1.700     48
        677.00   1.694     53
        675.05   1.690     43
        671.51   1.681     35
        668.58   1.673     32
        454.96   1.139     65
        452.76   1.133    138
        450.20   1.127    569
        447.75   1.121     87
        442.99   1.109   1000
        438.48   1.098     59
        435.67   1.091    500
    

in CDCl3



liquid film